C₁₇H₁₉NO

Base Information

• Chemical Name: C₁₇H₁₉NO
• CAS No.: 1221594-02-0
• Molecular Formula: C₁₇H₁₉NO
• Molecular Weight: 253.344
• Mol file: 1221594-02-0.mol

Synonyms:C₁₇H₁₉NO

Chemical Property of C₁₇H₁₉NO

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₇H₁₉NO

There total 1 articles about C₁₇H₁₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-(benzylamino)benzonitrile (5589-62-8) + isopropylmagnesium bromide (920-39-8) → C17H19NO (1221594-02-0)

Guidance literature:

2-(benzylamino)benzonitrile; isopropylmagnesium bromide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; methanol; at 0 ℃; Inert atmosphere;

With sodium hydroxide; In tetrahydrofuran; methanol; water; Inert atmosphere;

DOI:10.1016/j.tet.2010.01.073

Reference yield: 55.0%

C17H19NO (1221594-02-0) → 3,3-dimethyl-2-phenyl-2,3-dihydroquinolin-4(1H)-one + N-benzylanthranilic acid (6622-55-5)

Guidance literature:

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium tert-butylate; In dimethyl sulfoxide; at 20 - 80 ℃; for 6h;

DOI:10.1021/acs.orglett.5b00248

Reference yield:

C17H19NO (1221594-02-0) + Methyltriphenylphosphonium bromide (1779-49-3) → C18H21N

Guidance literature:

Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

C₁₇H₁₉NO; In tetrahydrofuran; hexane; at 0 - 40 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2010.01.073

upstream raw materials:

2-(benzylamino)benzonitrile

isopropylmagnesium bromide

Downstream raw materials:

N-benzylanthranilic acid

Refernces