4-AMINO-3,5,6-TRICHLORO-2-(TRICHLOROMETHYL)PYRIDINE

Base Information

• Chemical Name: 4-AMINO-3,5,6-TRICHLORO-2-(TRICHLOROMETHYL)PYRIDINE
• CAS No.: 5005-62-9
• Molecular Formula: C6H2Cl6N2
• Molecular Weight: 314.813
• Hs Code.: 2933399090
• Mol file: 5005-62-9.mol

Synonyms:4-Amino-3,5,6-Trichloro-2-(Trichloromethyl)Pyridine;

Chemical Property of 4-AMINO-3,5,6-TRICHLORO-2-(TRICHLOROMETHYL)PYRIDINE

Chemical Property:

• Vapor Pressure: 1.17E-05mmHg at 25°C
• Refractive Index: 1.643
• Boiling Point: 369.7 °C at 760 mmHg
• Flash Point: 177.4 °C
• PSA: 38.91000
• Density: 1.829 g/cm³
• LogP: 5.03190

Purity/Quality:

99% ^*data from raw suppliers

2,3,5-Trichloro-6-(trichloromethyl)pyridin-4-amine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AMINO-3,5,6-TRICHLORO-2-(TRICHLOROMETHYL)PYRIDINE

There total 2 articles about 4-AMINO-3,5,6-TRICHLORO-2-(TRICHLOROMETHYL)PYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,5-tetrachloro-6-(trichloromethyl)-pyridine (1134-04-9) → 4-amino-3,5,6-trichloro-2-trichloromethylpyridine (5005-62-9) + 6-amino-3,4,5-trichloro-2-trichloromethylpyridine

Guidance literature:

With ammonia; In dimethyl sulfoxide; at 100 ℃; for 0.5h;

Reference yield:

→ 4-amino-3,5,6-trichloro-2-trichloromethylpyridine (5005-62-9)

Guidance literature:

3,4,5,6-Tetrachlor-2-trichlormethyl-pyridin in DMSO, Einleiten v. NH3, 95grad;

Reference yield: 88.3%

4-amino-3,5,6-trichloro-2-trichloromethylpyridine (5005-62-9) → 4-amino-2,3,5-trichloropyridine (28443-69-8) + picloram (1918-02-1)

Guidance literature:

With sulfuric acid; trichloroacetic acid; In water; at 110 ℃; for 10h;

upstream raw materials:

2,3,4,5-tetrachloro-6-(trichloromethyl)-pyridine

Downstream raw materials:

4-amino-2,3,5-trichloropyridine

picloram

Refernces