Technology Process of Quinoline-4-carbaldehyde
There total 23 articles about Quinoline-4-carbaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert-Butyl iodide; trifluoroacetic acid; iron(II) chloride;
In
dimethyl sulfoxide;
at 80 ℃;
for 6h;
Product distribution;
var. reagents; reaction with addition of I2, in the absence of t-BuI, FeCl2, CF3CO2H;
- Guidance literature:
-
With
nickel(II) chloride hexahydrate; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; caesium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
Schlenk technique;
Inert atmosphere;
Irradiation;
DOI:10.1002/anie.201610108
- Guidance literature:
-
With
1-methyl-1H-imidazole; [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrakis(acetonitrile)copper(I)tetrafluoroborate;
In
acetonitrile;
at 20 ℃;
for 3h;
DOI:10.1021/jacs.1c05224
Xi
