1-adamantane methyl iodide

Base Information

• Chemical Name: 1-adamantane methyl iodide
• CAS No.: 51849-10-6
• Molecular Formula: C₁₁H₁₇I
• Molecular Weight: 276.16
• Mol file: 51849-10-6.mol

Synonyms:1-adamantane methyl iodide

Chemical Property of 1-adamantane methyl iodide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-adamantane methyl iodide

There total 3 articles about 1-adamantane methyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-adamantanemethanol (770-71-8) → 1-adamantane methyl iodide (51849-10-6)

Guidance literature:

With phosphoric acid; phosphorus pentoxide; sodium iodide;

DOI:10.1021/jo00932a013

Reference yield:

1-Adamantanecarboxylic acid (828-51-3) → 1-adamantane methyl iodide (51849-10-6)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / Heating

2: H₃PO₄, P₂O₅, NaI

With lithium aluminium tetrahydride; phosphoric acid; phosphorus pentoxide; sodium iodide; In diethyl ether;

DOI:10.1021/jo00932a013

Reference yield:

→ 1-adamantane methyl iodide (51849-10-6)

Guidance literature:

3-OH-Homoadamantan (6), HI;

DOI:10.1021/ja00829a033

upstream raw materials:

1-adamantanemethanol

1-Adamantanecarboxylic acid

Downstream raw materials:

2-(adamant-1-yl)ethanol

α-1-Adamantylmethylsulfonyl-methylidentriphenylphosphoran

2-<<(1-adamantyl)methyl>amino>ethanol

Refernces

• 1、 De Fenza, Maria,D'Alonzo, Daniele,Esposito, Anna,Munari, Silvia,Loberto, Nicoletta,Santangelo, Alessandra,Lampronti, Ilaria,Tamanini, Anna,Rossi, Alice,Ranucci, Serena,De Fino, Ida,Bragonzi, Alessandra,Aureli, Massimo,Bassi, Rosaria,Tironi, Matteo,Lippi, Giuseppe,Gambari, Roberto,Cabrini, Giulio,Palumbo, Giovanni,Dechecchi, Maria Cristina,Guaragna, Annalisa. "Exploring the effect of chirality on the therapeutic potential of N-alkyl-deoxyiminosugars: anti-inflammatory response to Pseudomonas aeruginosa infections for application in CF lung disease". . p. 63 - 71. Retrieved 2019/05/10.