cyclohexylzinc iodide

Base Information

• Chemical Name: cyclohexylzinc iodide
• CAS No.: 121883-35-0
• Molecular Formula: C₆H₁₁Zn*I
• Molecular Weight: 275.448
• Mol file: 121883-35-0.mol

Synonyms:cyclohexylzinc iodide

Chemical Property of cyclohexylzinc iodide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of cyclohexylzinc iodide

There total 2 articles about cyclohexylzinc iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Cyclohexyl iodide (626-62-0) + zinc (7440-66-6) → cyclohexylzinc iodide (121883-35-0)

Guidance literature:

In tetrahydrofuran; not isolated, GLC;;

Reference yield:

Cyclohexyl iodide (626-62-0) → cyclohexylzinc iodide (121883-35-0)

Guidance literature:

With zinc; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1055/s-0039-1690127

Reference yield: 98.0%

(E)-1-bromo-1-octene (51751-87-2) + cyclohexylzinc iodide (121883-35-0) → (E)-(oct-1-en-1-yl)cyclohexane (87393-89-3)

Guidance literature:

With 1-methyl-1H-imidazole; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); In tetrahydrofuran; at 20 ℃; for 24h; stereoselective reaction; Inert atmosphere;

DOI:10.1021/ol201307y

upstream raw materials:

Cyclohexyl iodide

zinc

Downstream raw materials:

ethyl 4-cyclohexylbutanoate

cyclohexane carbonitrile

1-cyclohexyl-1-butanol

3-cyclohexylcyclohexanone

Refernces

• 1、 -. "3,6-DIAMINO-PYRIDAZIN-3-YL DERIVATIVES, PHARMACEUTICAL COMPOSITIONS CONTAINING THEM AND THEIR USES AS PRO-APOPTOTIC AGENTS". Page/Page column 349-350. . Retrieved 2021/02/05.
• 2、 Rauser, Marian,Ascheberg, Christoph,Niggemann, Meike. "Direct Reductive N-Functionalization of Aliphatic Nitro Compounds". supporting information. p. 3970 - 3974. Retrieved 2018/02/26.