Technology Process of C20H18O8*C28H34BrNO
There total 7 articles about C20H18O8*C28H34BrNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
isopropyl alcohol;
at 25 - 86 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid / 120 - 125 °C
2.1: potassium carbonate; sodium iodide / acetone / Reflux
3.1: sodium tetrahydroborate / 1,2-dimethoxyethane / 0.17 h
3.2: 3 h / 10 °C
4.1: triethylamine / dichloromethane / 12 h / 25 - 30 °C
5.1: acetonitrile / 30 h / 95 - 100 °C / autoclave; Sealed tube
6.1: isopropyl alcohol / 15 h / 25 - 86 °C
With
sodium tetrahydroborate; sulfuric acid; potassium carbonate; triethylamine; sodium iodide;
In
1,2-dimethoxyethane; dichloromethane; isopropyl alcohol; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 12 h / 25 - 30 °C
2: acetonitrile / 30 h / 95 - 100 °C / autoclave; Sealed tube
3: isopropyl alcohol / 15 h / 25 - 86 °C
With
triethylamine;
In
dichloromethane; isopropyl alcohol; acetonitrile;
