Technology Process of 17-Deoxyestradiol
There total 21 articles about 17-Deoxyestradiol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethyl acetate;
at 20 ℃;
for 3h;
under 15001.5 Torr;
DOI:10.1016/j.steroids.2016.05.010
- Guidance literature:
-
With
bismuth(III) oxide; N-ethyl-N,N-diisopropylamine; para-thiocresol;
In
dichloromethane;
for 2h;
Irradiation;
- Guidance literature:
-
Estrone;
With
hydrazine hydrate; potassium hydroxide;
In
butan-1-ol; diethylene glycol;
for 0.5h;
Reflux;
In
water; butan-1-ol;
at 200 ℃;
for 2h;
DOI:10.1021/acs.joc.9b00786
