Dioleamide

Base Information

• Chemical Name: Dioleamide
• CAS No.: 72901-31-6
• Molecular Formula: C₃₆H₆₉NO
• Molecular Weight: 531.95
• European Community (EC) Number: 276-974-8
• Mol file: 72901-31-6.mol

Synonyms:Dioleamide;Oleyl oleamide;EINECS 276-974-8;9-Octadecenamide, N-(9Z)-9-octadecen-1-yl-, (9Z)-;72901-31-6;9-Octadecenamide, N-(9Z)-9-octadecenyl-, (9Z)-;C36H69NO;C36-H69-N-O;9-Octadecenamide, N-9-octadecenyl-, (Z,Z)-

Chemical Property of Dioleamide

Chemical Property:

• Vapor Pressure: 2.6E-16mmHg at 25°C
• Melting Point: 45℃
• Boiling Point: 640.7°C at 760 mmHg
• Flash Point: 398.3°C
• PSA: 29.10000
• Density: 0.863g/cm³
• LogP: 12.56850
• Water Solubility.: 0ng/L at 25℃
• XLogP3: 14.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 31
• Exact Mass: 531.53791582
• Heavy Atom Count: 38
• Complexity: 510

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCC=CCCCCCCCCNC(=O)CCCCCCCC=CCCCCCCCC
• Isomeric SMILES: CCCCCCCC/C=C/CCCCCCCCNC(=O)CCCCCCC/C=C\CCCCCCCC

Technology Process of Dioleamide

There total 2 articles about Dioleamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(Z)-9-octadecenoyl chloride (112-77-6) + (Z)-9-octadecen-1-amine (112-90-3) → (9Z)-N-[(9Z)-9-octadecen-1-yl]-9-octadecenamide (72901-31-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 21h;

DOI:10.1021/acs.jmedchem.5b01679

Reference yield: 88.0%

(Z)-9-octadecen-1-amine (112-90-3) + cis-Octadecenoic acid (112-80-1,2027-47-6) → (9Z)-N-[(9Z)-9-octadecen-1-yl]-9-octadecenamide (72901-31-6)

Guidance literature:

With ethanol; at 160 ℃; for 6h; Temperature; Reagent/catalyst; Concentration; Time; Autoclave; Green chemistry;

DOI:10.1039/c7gc02967e

upstream raw materials:

(Z)-9-octadecen-1-amine

cis-Octadecenoic acid

(Z)-9-octadecenoyl chloride

Refernces

• 1、 Dalu, Francesca,Scorciapino, Mariano A.,Cara, Claudio,Luridiana, Alberto,Musinu, Anna,Casu, Mariano,Secci, Francesco,Cannas, Carla. "A catalyst-free, waste-less ethanol-based solvothermal synthesis of amides". supporting information. p. 375 - 381. Retrieved 2018/02/07.