Technology Process of C22H16F6O2
There total 4 articles about C22H16F6O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
1-methyl-pyrrolidin-2-one;
at 90 ℃;
for 31h;
Inert atmosphere;
DOI:10.1021/ma2028209
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 27 h / Reflux
2: potassium carbonate / 1-methyl-pyrrolidin-2-one / 31 h / 90 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1-methyl-pyrrolidin-2-one; ethanol; water; toluene;
DOI:10.1021/ma2028209
- Guidance literature:
-
Multi-step reaction with 3 steps
1: disodium hydrogenphosphate; Oxone; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / dichloromethane; water; acetone / 0.5 h / 0 °C / pH 7.5 - 8.5 / aq. phosphate buffer
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 27 h / Reflux
3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 31 h / 90 °C / Inert atmosphere
With
disodium hydrogenphosphate; tetrakis(triphenylphosphine) palladium(0); Oxone; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide;
In
1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; water; acetone; toluene;
DOI:10.1021/ma2028209
