2-Methyl-4-(dimethylamino)azobenzene

Base Information

• Chemical Name: 2-Methyl-4-(dimethylamino)azobenzene
• CAS No.: 54-88-6
• Molecular Formula: C15H17 N3
• Molecular Weight: 239.32
• Hs Code.: 2927000090
• European Community (EC) Number: 200-217-2
• NSC Number: 102372
• UNII: 25Q2BUE0AS
• DSSTox Substance ID: DTXSID0074845
• Nikkaji Number: J2.800B
• Wikidata: Q27253984
• Mol file: 54-88-6.mol

Synonyms:2-methyl-4-dimethylaminoazobenzene

Chemical Property of 2-Methyl-4-(dimethylamino)azobenzene

Chemical Property:

• Appearance/Colour: orange crystalline solid
• Vapor Pressure: 2.57E-06mmHg at 25°C
• Melting Point: 67-69 °C(lit.)
• Refractive Index: 1.5610 (estimate)
• Boiling Point: 150 °C / 16mmHg
• PKA: 3.68(at 25℃)
• Flash Point: 190.2°C
• PSA: 27.96000
• Density: 1.01g/cm³
• LogP: 4.47640
• Solubility.: Solubility Practically insoluble in water; soluble in ethanol, a
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 239.142247555
• Heavy Atom Count: 18
• Complexity: 269

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-?Dimethylamino-?2-?methylazobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-40
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)N(C)C)N=NC2=CC=CC=C2

Technology Process of 2-Methyl-4-(dimethylamino)azobenzene

There total 2 articles about 2-Methyl-4-(dimethylamino)azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-m-toluidine (121-72-2) + aniline (62-53-3) → 2-methyl-4-dimethylaminoazobenzene (54-88-6)

Guidance literature:

With hydrogenchloride; sodium hydroxide; sodium nitrite; Reagens 4: Wasser;

Reference yield:

N,N-dimethyl-m-toluidine (121-72-2) + water (7732-18-5) + aniline hydrochloride (142-04-1,36663-09-9) → 2-methyl-4-dimethylaminoazobenzene (54-88-6)

Guidance literature:

upstream raw materials:

N,N-dimethyl-m-toluidine

aniline

water

aniline hydrochloride