Cyclohexene, 1-cyclohexyl-

Base Information

• Chemical Name: Cyclohexene, 1-cyclohexyl-
• CAS No.: 3282-54-0
• Molecular Formula: C12H20
• Molecular Weight: 164.291
• Hs Code.: 2902199090
• DSSTox Substance ID: DTXSID20186496
• Nikkaji Number: J661.261J
• Wikidata: Q83057797
• Mol file: 3282-54-0.mol

Synonyms:1-cyclohexylcyclohexene;Cyclohexene, 1-cyclohexyl-;3282-54-0;Cyclohexene,1-cyclohexyl-;1-Cyclohexyl-1-cyclohexene;1-CYCLOHEXYLCYCLOHEX-1-ENE;cyclohexylcyclohexene;1-Cyclohexyl-1-cyclohexene #;DTXSID20186496;RFFCUDDJJDOFLS-UHFFFAOYSA-N;AKOS006272376;FT-0697123

Chemical Property of Cyclohexene, 1-cyclohexyl-

Chemical Property:

• Melting Point: -43 °C
• Boiling Point: 234.2°Cat760mmHg
• Flash Point: 90°C
• PSA: 0.00000
• Density: 0.923g/cm³
• LogP: 4.06710
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 164.156500638
• Heavy Atom Count: 12
• Complexity: 161

Purity/Quality:

98%Min ^*data from raw suppliers

1-CYCLOHEXYLCYCLOHEXENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)C2=CCCCC2

Technology Process of Cyclohexene, 1-cyclohexyl-

There total 61 articles about Cyclohexene, 1-cyclohexyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-cyclohexyl-1-cyclohexene (3282-54-0)

Guidance literature:

With titanium(III) chloride; In 1,2-dimethoxyethane; for 3h;

DOI:10.1021/jo00022a042

Reference yield: 53.0%

1-cyclohexylcyclohexanol (2903-12-0) → 1-cyclohexyl-1-cyclohexene (3282-54-0)

Guidance literature:

With dmap; bis(trichloromethyl) carbonate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/acs.orglett.9b01959

Reference yield: 29.0%

cyclohexene (110-83-8) → 1-cyclohexyl-1-cyclohexene (3282-54-0)

Guidance literature:

With NH₄F/Al₂O₃; at 83 ℃; for 6h;

DOI:10.1016/j.mencom.2013.03.021

upstream raw materials:

pyridine

1-bromo-bicyclohexyl

methanol

biphenyl

Downstream raw materials:

cyclohexylcyclohexane

6-cyclohexyl-6-oxohexanoic acid

6-Acetoxy-1-cyclohexyl-cyclohexen-⁽¹⁾

cyclohexyl(cyclopentyl)methanone

Refernces

• 1、 Szymanska, Agnieszka,Lewandowski, Marek,Sayag, Celine,Djega-Mariadassou, Gerald. "Kinetic study of the hydrodenitrogenation of carbazole over bulk molybdenum carbide". . p. 24 - 31. Retrieved 2003.
• 2、 Dong, Peng,Lu, Guo-Ping,Cai, Chun. "Effective hydrodeoxygenation of dibenzofuran by a bimetallic catalyst in water". . p. 1605 - 1609. Retrieved 2016/02/19.