4--1-methyl-5-methylaminocarbonylimidazole

Base Information

• Chemical Name: 4--1-methyl-5-methylaminocarbonylimidazole
• CAS No.: 107605-83-4
• Molecular Formula: C₁₈H₂₀N₄O₃
• Molecular Weight: 340.382
• Mol file: 107605-83-4.mol

Synonyms:4--1-methyl-5-methylaminocarbonylimidazole

Chemical Property of 4--1-methyl-5-methylaminocarbonylimidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4--1-methyl-5-methylaminocarbonylimidazole

There total 2 articles about 4--1-methyl-5-methylaminocarbonylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4--1-methyl-5-methylaminocarbonylimidazole (107605-82-3) + benzyl alcohol (100-51-6,185532-71-2) → 4--1-methyl-5-methylaminocarbonylimidazole (107605-83-4)

Guidance literature:

With piperidine; benzoic acid; In benzene; for 2h; Heating;

DOI:10.1248/cpb.34.3573

Reference yield:

caffeidine (20041-90-1) → 4--1-methyl-5-methylaminocarbonylimidazole (107605-83-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / Et₃N / CHCl₃ / 1 h / Heating

2: 75 percent / piperidine, benzoic acid / benzene / 2 h / Heating

With piperidine; triethylamine; benzoic acid; In chloroform; benzene;

DOI:10.1248/cpb.34.3573

Reference yield: 81.0%

4--1-methyl-5-methylaminocarbonylimidazole (107605-83-4) → 3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione (58-08-2,138455-22-8,95789-13-2)

Guidance literature:

With sodium hydride; In ethanol; for 1.5h; Heating;

DOI:10.1248/cpb.34.3573

upstream raw materials:

4--1-methyl-5-methylaminocarbonylimidazole

benzyl alcohol

caffeidine

Downstream raw materials:

3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione

1-methyl-5-methylaminocarbonyl-4-(N-cinnamoyl-N-methylamino)imidazole

Refernces