2'-Nitroacetophenone

Base Information Edit

Chemical Name:2'-Nitroacetophenone
CAS No.:577-59-3
Molecular Formula:C8H7NO3
Molecular Weight:165.148
Hs Code.:29147090
European Community (EC) Number:209-414-8
NSC Number:3641
UNII:52L53K4X3O
DSSTox Substance ID:DTXSID6025723
Nikkaji Number:J835D
Wikidata:Q27261014
ChEMBL ID:CHEMBL1881120
Mol file:577-59-3.mol

Synonyms:2'-Nitroacetophenone;577-59-3;1-(2-Nitrophenyl)ethanone;O-NITROACETOPHENONE;2-Acetylnitrobenzene;Ethanone, 1-(2-nitrophenyl)-;Acetophenone, 2'-nitro-;Methyl 2-nitrophenyl ketone;CCRIS 2329;1-(2-Nitrophenyl)ethan-1-one;NSC 3641;EINECS 209-414-8;MFCD00007144;BRN 1102322;UNII-52L53K4X3O;DTXSID6025723;52L53K4X3O;NSC-3641;4-07-00-00655 (Beilstein Handbook Reference);1-acetyl-2-nitrobenzene;o-nitroacetophenon;NSC3641;2`-Nitroacetophenone;2'-nitro-acetophenone;1-(2-nitrophenyl)-ethanone;2'-Nitroacetophenone, 95%;NITROACETOPHENONE, O-;MLS002415763;SCHEMBL334763;1-(2-nitro-phenyl)-ethanone;CCRIS-2329;DTXCID705723;CHEMBL1881120;SCHEMBL14438210;METHYL O-NITROPHENYL KETONE;STR04123;Tox21_200072;AKOS000120648;AC-2890;AM10565;CS-W017892;LS-1406;PS-3008;NCGC00091366-01;NCGC00091366-02;NCGC00257626-01;CAS-577-59-3;SMR001261211;SY003270;A8223;FT-0613171;N0110;2 inverted exclamation mark -Nitroacetophenone;EN300-20910;W-105443;Q27261014;F0001-1504

Suppliers and Price of 2'-Nitroacetophenone

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2''-Nitroacetophenone
100g
$ 365.00

TCI Chemical
2'-Nitroacetophenone >96.0%(GC)
5g
$ 17.00

TCI Chemical
2'-Nitroacetophenone >96.0%(GC)
25g
$ 48.00

SynQuest Laboratories
2'-Nitroacetophenone
10 g
$ 18.00

SynQuest Laboratories
2'-Nitroacetophenone
100 g
$ 90.00

SynQuest Laboratories
2'-Nitroacetophenone
25 g
$ 30.00

Sigma-Aldrich
2′-Nitroacetophenone 95%
10g
$ 73.30

Sigma-Aldrich
2′-Nitroacetophenone 95%
25g
$ 69.00

Sigma-Aldrich
2′-Nitroacetophenone 95%
1g
$ 22.60

Matrix Scientific
1-(2-Nitrophenyl)ethanone 95+%
10g
$ 11.00

Total 113 raw suppliers

Chemical Property of 2'-Nitroacetophenone Edit

Chemical Property:

Appearance/Colour:yellow-green liquid or crystal
Vapor Pressure:0.00126mmHg at 25°C
Melting Point:76-78 °C(lit.)
Refractive Index:n20/D 1.55(lit.)
Boiling Point:286.4 °C at 760 mmHg
Flash Point:137.8 °C
PSA：62.89000
Density:1.243 g/cm³
LogP:2.32060
Storage Temp.:Refrigerator
Solubility.:Chloroform, Ethyl Acetate
Water Solubility.:Insoluble
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:165.042593085
Heavy Atom Count:12
Complexity:197

Purity/Quality:

99% ^*data from raw suppliers

2''-Nitroacetophenone ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22
Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC(=O)C1=CC=CC=C1[N+](=O)[O-]
Uses 2'-Nitroacetophenone is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and dyestuff. It is also used as a synthetic reagent. It is the sensitizer which can be used as pharmaceutical intermediates. 2''-Nitroacetophenone (cas# 577-59-3) is a compound useful in organic synthesis. It is also used as an intermediate for photosensitive materials.?

Technology Process of 2'-Nitroacetophenone

There total 63 articles about 2'-Nitroacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98-86-2
acetophenone

: 577-59-3
2-acetylnitrobenzene

Guidance literature:: With calcium silicate; sulfuric acid; nitric acid; at -15 ℃;

Reference yield: 96.0%

: 612-22-6
2-nitro(ethylbenzene)

: 577-59-3
2-acetylnitrobenzene

Guidance literature:: With potassium permanganate; sulfuric acid; acetic acid; In water; at 30 - 50 ℃; for 8h; Temperature; Reagent/catalyst; Cooling; Large scale;

Reference yield: 96.0%

: 80379-10-8,108530-03-6,142631-59-2,3205-25-2
1-(2-nitrophenyl)ethan-1-ol

: 577-59-3
2-acetylnitrobenzene

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; iron(III) chloride; In water; ethyl acetate; at 20 ℃; for 10h;
DOI:10.1139/V08-059