2-(2,5-dimethylphenoxymethyl)benzal chloride

Base Information

• Chemical Name: 2-(2,5-dimethylphenoxymethyl)benzal chloride
• CAS No.: 1182310-82-2
• Molecular Formula: C₁₆H₁₆Cl₂O
• Molecular Weight: 295.208
• Mol file: 1182310-82-2.mol

Synonyms:2-(2,5-dimethylphenoxymethyl)benzal chloride

Chemical Property of 2-(2,5-dimethylphenoxymethyl)benzal chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(2,5-dimethylphenoxymethyl)benzal chloride

There total 1 articles about 2-(2,5-dimethylphenoxymethyl)benzal chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-Dimethylphenol (95-87-4) + α,α,α'-trichloro-o-xylene (30293-58-4) → 2-(2,5-dimethylphenoxymethyl)benzal chloride (1182310-82-2)

Guidance literature:

2,5-Dimethylphenol; With sodium hydroxide; In water; toluene; at 20 - 80 ℃;

α,α,α'-trichloro-o-xylene; With tetrabutylammomium bromide; In toluene; at 40 ℃;

Reference yield: 99.1%

methanol (67-56-1) + 2-(2,5-dimethylphenoxymethyl)benzal chloride (1182310-82-2) + sodium methylate (124-41-4) → 2-(2,5-dimethylphenoxymethyl)benzaldehyde dimethyl acetal (1182310-78-6)

Guidance literature:

at 80 - 85 ℃; for 23h;

Reference yield:

2-(2,5-dimethylphenoxymethyl)benzal chloride (1182310-82-2) → 2-(2,5-dimethylphenoxymethyl)benzaldehyde (1086328-92-8)

Guidance literature:

2-(2,5-dimethylphenoxymethyl)benzal chloride; With methanol; sodium methylate; at 80 - 85 ℃; for 47h;

With sulfuric acid; In methanol; water; xylene; at 60 ℃; for 2h;

upstream raw materials:

2,5-Dimethylphenol

α,α,α'-trichloro-o-xylene

Downstream raw materials:

2-(2,5-dimethylphenoxymethyl)benzaldehyde dimethyl acetal

2-(2,5-dimethylphenoxymethyl)benzaldehyde

2-(2,5-dimethylphenoxymethyl)benzaldehyde ethylene glycol acetal

Refernces

• 1、 -. "PROCESS FOR PRODUCTION OF BENZALDEHYDE COMPOUND". Page/Page column 10. . Retrieved 2011/04/25.