Technology Process of Dibenzylamine hydrochloride
There total 21 articles about Dibenzylamine hydrochloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloroform; 10% Pd/C; hydrogen;
In
methanol;
at 20 ℃;
for 2h;
under 760.051 Torr;
chemoselective reaction;
DOI:10.1016/j.tet.2008.09.072
- Guidance literature:
-
N-benzylbenzamide;
With
dodecacarbonyl-triangulo-triruthenium; 1,1,3,3-tetramethyldisilazane;
In
toluene;
at 20 - 50 ℃;
for 24.17h;
Inert atmosphere;
With
hydrogenchloride;
In
1,4-dioxane; ethyl acetate; toluene;
at 20 ℃;
for 0.5h;
DOI:10.1002/adsc.201200835
- Guidance literature:
-
With
aluminum oxide; silica gel; potassium carbonate;
sodium percarbonate; sodium salt of 2,4-dichloro-6-hydroxy-1,3,5-triazine;
In
chloroform;
column chromatography;
DOI:10.1021/ol036319g