H₂NC₂HN₃SSn(CH₂C₆H₅)3

Base Information

• Chemical Name: H₂NC₂HN₃SSn(CH₂C₆H₅)3
• CAS No.: 1005198-29-7
• Molecular Formula: C₂₃H₂₄N₄SSn
• Molecular Weight: 507.246
• Mol file: 1005198-29-7.mol

Synonyms:H₂NC₂HN₃SSn(CH₂C₆H₅)3

Chemical Property of H₂NC₂HN₃SSn(CH₂C₆H₅)3

Chemical Property:

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Technology Process of H₂NC₂HN₃SSn(CH₂C₆H₅)3

There total 1 articles about H₂NC₂HN₃SSn(CH₂C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

tribenzyltin(IV) chloride (3151-41-5) + 5-amino-3-mercapto-4H-[1,2,4]triazole (16691-43-3) → H2NC2HN3SSn(CH2C6H5)3 (1005198-29-7)

Guidance literature:

With EtONa; In benzene; (N2); stoich. mixt. ligand and EtONa in benzene stirred for 0.5 h, Sn compd. (1 equiv.) added, stirred for 12 h at 40°C; cooled to room temp., filtered, evapd., recrystd. (Et2O); elem. anal.;

DOI:10.1016/j.ica.2007.06.045

upstream raw materials:

tribenzyltin(IV) chloride

5-amino-3-mercapto-4H-[1,2,4]triazole

Refernces