2-(3,4-methylenedioxyphenyl)-1-phenylethanamine

Base Information

• Chemical Name: 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine
• CAS No.: 179397-86-5
• Molecular Formula: C₁₅H₁₅NO₂
• Molecular Weight: 241.29
• Mol file: 179397-86-5.mol

Synonyms:2-(3,4-methylenedioxyphenyl)-1-phenylethanamine

Chemical Property of 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine

There total 5 articles about 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

trans-1-(3,4-methylenedioxyphenyl)-2-phenylethylene (51003-16-8,5426-80-2) → 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine (179397-86-5)

Guidance literature:

With terephthalonitrile; ammonia; In water; acetonitrile; benzene; for 20h; Ambient temperature; Irradiation;

DOI:10.1021/jo00031a010

Reference yield:

→ 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine (179397-86-5)

Guidance literature:

With alkaline aqueous sodium hypochlorite solution;

Reference yield:

3,4-methylenedioxy-α'-nitro-trans-stilbene (50882-25-2) → 2-(3,4-methylenedioxyphenyl)-1-phenylethanamine (179397-86-5)

Guidance literature:

With sulfuric acid; acetic acid; platinum; Hydrogenation;

DOI:10.1021/ja01208a028 DOI:10.1002/ardp.19362740901

upstream raw materials:

3,4-methylenedioxy-α'-nitro-trans-stilbene

trans-1-(3,4-methylenedioxyphenyl)-2-phenylethylene

2-(benzo[d][1,3]dioxol-5-yl)-1-phenylethan-1-one

Downstream raw materials:

(R)-1-phenyl-2-(benzo[1,3]dioxol-5-yl)-ethylammonium D-aspartate

(S)-1-phenyl-2-(benzo[1,3]dioxol-5-yl)-ethylammonium L-aspartate

Refernces

• 1、 Yasuda, Masahide,Isami, Toshihiro,Kubo, Jun-ichi,Mizutani, Manabu,Yamashita, Toshiaki,et al.. "Regiochemistry on Photoamination of Stilbene Derivatives with Ammonia via Electron Transfer". . p. 1351 - 1354. Retrieved 2007/10/02.