4-cyano-1,3-phenylene diacetate

Base Information Edit

Chemical Name:4-cyano-1,3-phenylene diacetate
CAS No.:197571-05-4
Molecular Formula:C₁₁H₉NO₄
Molecular Weight:219.197
Hs Code.:
Mol file:197571-05-4.mol

Synonyms:4-cyano-1,3-phenylene diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-cyano-1,3-phenylene diacetate Edit

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Technology Process of 4-cyano-1,3-phenylene diacetate

There total 3 articles about 4-cyano-1,3-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 5399-68-8
2,4-dihydroxyphenylaldoxime

: 108-24-7
acetic anhydride

: 197571-05-4
4-cyano-1,3-phenylene diacetate

Guidance literature:: for 8h; Reflux;
DOI:10.1016/j.bmc.2015.01.003

Reference yield:

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 197571-05-4
4-cyano-1,3-phenylene diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; potassium hydroxide / water; ethanol / 0.5 h / 0 °C / Reflux

2: 8 h / Reflux

With hydroxylamine hydrochloride; potassium hydroxide; In ethanol; water;
DOI:10.1016/j.bmc.2015.01.003