Technology Process of XENON HEXAFLUORIDE
There total 21 articles about XENON HEXAFLUORIDE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
NaF;
byproducts: CF4; NaF dried at 900°C, filled in HP-autoclave, Xe and F2 condensed at -196°C, mixt. warmed at 250°C for 1 d, excess of F2, XeF4, XeOF4 and CF4 removed in vac., Na2XeF8 (residue) warmed to 50-100°C, XeF6 recovered in vac.;
- Guidance literature:
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In
neat (no solvent);
immersing of a hot wire reactor in liquid N2 which is connected to a vac. system and heating of the Ni-filament to 700-800°C (dc power), condensing of Xe onto the walls, introducing of excess of F2 (160 Torr), heating to 700-800°C for 1 h; condensing of solid at -78°C into a stainless trap, detected by IR;
- Guidance literature:
-
In
neat (no solvent);
thermolysis; mass spectrum of gas phase at 197 to 335°C, identification of residue (Mn2F5) by X-ray diffraction and elem. anal.;
