Technology Process of C32H23NO4
There total 3 articles about C32H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trichlorophosphate;
In
1,2-dichloro-ethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1007/s11426-011-4248-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: trichlorophosphate / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere
With
potassium tert-butylate; trichlorophosphate;
In
tetrahydrofuran; 1,2-dichloro-ethane;
1.2: Wittig-Horner-Emmons olefination / 2.1: Vilsmeier reaction;
DOI:10.1007/s11426-011-4248-4
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 40 °C
2.1: iodine / 0 - 20 °C
3.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: trichlorophosphate / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere
With
sodium tetrahydroborate; potassium tert-butylate; iodine; trichlorophosphate;
In
tetrahydrofuran; ethanol; 1,2-dichloro-ethane;
3.2: Wittig-Horner-Emmons olefination / 4.1: Vilsmeier reaction;
DOI:10.1007/s11426-011-4248-4
