Phenyl 1-hydroxy-2-naphthoate

Base Information

• Chemical Name: Phenyl 1-hydroxy-2-naphthoate
• CAS No.: 132-54-7
• Molecular Formula: C17H12O3
• Molecular Weight: 264.28
• Hs Code.: 29182900
• European Community (EC) Number: 205-065-0
• NSC Number: 1867
• UNII: 0749HK9B6B
• DSSTox Substance ID: DTXSID1038876
• Nikkaji Number: J167.288F
• Wikidata: Q27236257
• ChEMBL ID: CHEMBL3186248
• Mol file: 132-54-7.mol

Synonyms:Phenyl 1-hydroxy-2-naphthoate;132-54-7;1-Hydroxy-2-naphthoic acid phenyl ester;phenyl 1-hydroxynaphthalene-2-carboxylate;2-Naphthalenecarboxylic acid, 1-hydroxy-, phenyl ester;Phenyl 1-hydroxy-2-naphthalenecarboxylate;C17H12O3;phenyl-1-hydroxy-2-naphthate;2-phenoxycarbonyl-1-naphthol;UNII-0749HK9B6B;2-Naphthoic acid, 1-hydroxy-, phenyl ester;DTXSID1038876;0749HK9B6B;NSC 1867;NSC-1867;EINECS 205-065-0;Oprea1_599311;SCHEMBL27607;Phenyl1-hydroxy-2-naphthoate;1-hydroxy-2-naphthalenecarboxylic acid phenyl ester;phenyl-1-hydroxy-2-naphthoat;2-Naphthoic acid, phenyl ester;CHEMBL3186248;DTXCID9018876;QHDYIMWKSCJTIM-UHFFFAOYSA-;NSC1867;Tox21_301650;MFCD00014310;STK392173;AKOS003245262;Phenyl 1-hydroxy-2-naphthoate, 99%;PHENYL 1-HYDROXY-2-NAPHTHALATE;NCGC00255458-01;AC-13238;AS-69564;CAS-132-54-7;2-Naphthalenecarboxylic acid, phenyl ester;CS-0156094;FT-0631768;H0797;S12375;A806456;W-108314;Q27236257

Chemical Property of Phenyl 1-hydroxy-2-naphthoate

Chemical Property:

• Appearance/Colour: almost white to greenish-beige crystalline powder
• Vapor Pressure: 9.27E-08mmHg at 25°C
• Melting Point: 94-96 °C(lit.)
• Refractive Index: 1.68
• Boiling Point: 423.2 °C at 760 mmHg
• PKA: 7.71±0.50(Predicted)
• Flash Point: 179.8 °C
• PSA: 46.53000
• Density: 1.286 g/cm³
• LogP: 3.76460
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 264.078644241
• Heavy Atom Count: 20
• Complexity: 335

Purity/Quality:

99% ^*data from raw suppliers

Phenyl 1-hydroxy-2-naphthoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36-37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)OC(=O)C2=C(C3=CC=CC=C3C=C2)O

Technology Process of Phenyl 1-hydroxy-2-naphthoate

There total 3 articles about Phenyl 1-hydroxy-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-naphthol (90-15-3) + phenyl chloroformate (1885-14-9) → phenyl 1-hydroxy-2-naphthoate (132-54-7)

Guidance literature:

With hydrogenchloride; aluminium trichloride; In water; toluene;

Reference yield:

phenol (108-95-2,27073-41-2) + 1-hydroxy-2-naphthoic acid (86-48-6) → phenyl 1-hydroxy-2-naphthoate (132-54-7)

Guidance literature:

With trichlorophosphate; at 120 ℃;

Reference yield:

→ phenyl 1-hydroxy-2-naphthoate (132-54-7)

Guidance literature:

1-Hydroxy-naphthoesaeure-2, Phenol (1 Mol), Xylol od. Bzl., POCl3 od. PCl3 od. P2O5, 110grad-120grad;

DOI:10.1016/0040-4020(66)80143-6

upstream raw materials:

phenol

1-hydroxy-2-naphthoic acid

α-naphthol

phenyl chloroformate

Downstream raw materials:

benzenesulfonyl-(1-hydroxy-[2]naphthoyl)-amine

1-hydroxy-[2]naphthoic acid-(2-dimethylamino-anilide)

1-hydroxy-[2]naphthoic acid-[2-chloro-4-(1-methyl-butyl)-anilide]

5-(2,4-bis-methoxycarbonylmethoxy-benzoylamino)-2-(2,4-di-tert-pentyl-phenoxy)-benzoic acid-{4-[2-(1-hydroxy-[2]naphthoylamino)-ethyl]-anilide}

Refernces