Technology Process of C26H34O3S2Si
There total 6 articles about C26H34O3S2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
toluene;
at -78 ℃;
for 0.5h;
Yield given;
DOI:10.1021/ja00344a047
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 4-(dimethylamino)pyridine / CH2Cl2 / 0.5 h / 0 °C
2: K2CO3 / methanol / 1.5 h / 23 °C
3: 90 percent / diisopropylcarbodiimide, dichloroacetic acid / benzene; dimethylsulfoxide / 0.5 h / 23 °C
4: zinc triflate / CH2Cl2 / 5 h / 23 °C
5: diisobutylaluminum hydride / toluene / 0.5 h / -78 °C
With
dichloro-acetic acid; dmap; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; potassium carbonate; diisopropyl-carbodiimide;
In
methanol; dichloromethane; dimethyl sulfoxide; toluene; benzene;
DOI:10.1021/ja00344a047
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) trimethylchlorosilane, NaI / 1.) MeCN, 50 deg C, 4 h
2: 4-(dimethylamino)pyridine / CH2Cl2 / 0.5 h / 0 °C
3: K2CO3 / methanol / 1.5 h / 23 °C
4: 90 percent / diisopropylcarbodiimide, dichloroacetic acid / benzene; dimethylsulfoxide / 0.5 h / 23 °C
5: zinc triflate / CH2Cl2 / 5 h / 23 °C
6: diisobutylaluminum hydride / toluene / 0.5 h / -78 °C
With
dichloro-acetic acid; dmap; chloro-trimethyl-silane; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; potassium carbonate; sodium iodide; diisopropyl-carbodiimide;
In
methanol; dichloromethane; dimethyl sulfoxide; toluene; benzene;
DOI:10.1021/ja00344a047
