Methanol, (butylmethylsilylene)di-, dicarbamate (ester)

Base Information

• Chemical Name: Methanol, (butylmethylsilylene)di-, dicarbamate (ester)
• CAS No.: 3124-49-0
• Molecular Formula: C₉H₂₀N₂O₄Si
• Molecular Weight: 248.354
• NSC Number: 96878
• DSSTox Substance ID: DTXSID40185168
• Wikidata: Q83056154
• Mol file: 3124-49-0.mol

Synonyms:Methanol, (butylmethylsilylene)di-, dicarbamate (ester);3124-49-0;BRN 2416988;(Butylmethylsilylene)dimethanol carbamate;Carbamic acid, (butylmethylsilylene)dimethylene ester;(Butylmethylsilylene)dimethylene ester of carbamic acid;DTXSID40185168;NSC96878;NSC 96878;NSC-96878

Chemical Property of Methanol, (butylmethylsilylene)di-, dicarbamate (ester)

Chemical Property:

• Vapor Pressure: 9.03E-08mmHg at 25°C
• Boiling Point: 435°C at 760 mmHg
• Flash Point: 216.9°C
• Density: 1.093g/cm³
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 248.11923366
• Heavy Atom Count: 16
• Complexity: 230

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[Si](C)(COC(=O)N)COC(=O)N

Technology Process of Methanol, (butylmethylsilylene)di-, dicarbamate (ester)

There total 3 articles about Methanol, (butylmethylsilylene)di-, dicarbamate (ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Bis-chlormethyl)-butyl-methylsilan (2917-66-0) → Dicarbamat des Butyl-(bis-hydroxymethyl)-methyl-silans (3124-49-0)

Guidance literature:

Multi-step reaction with 3 steps

1: KOAc

2: LiAlH₄

3: (i) Py, (ii) liq. NH₃

With lithium aluminium tetrahydride; potassium acetate;

DOI:10.1021/jm00329a012

Reference yield:

(Bis-acetoxymethyl)-butyl-methylsilan (2917-58-0) → Dicarbamat des Butyl-(bis-hydroxymethyl)-methyl-silans (3124-49-0)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

2: (i) Py, (ii) liq. NH₃

With lithium aluminium tetrahydride;

DOI:10.1021/jm00329a012

Reference yield:

Butyl-(bis-hydroxymethyl)-methylsilan (2917-50-2) + phenyl chloroformate (1885-14-9) → Dicarbamat des Butyl-(bis-hydroxymethyl)-methyl-silans (3124-49-0)

Guidance literature:

Multistep reaction; (i) Py, (ii) liq. NH₃;

DOI:10.1021/jm00329a012

upstream raw materials:

Butyl-(bis-hydroxymethyl)-methylsilan

phenyl chloroformate

(Bis-chlormethyl)-butyl-methylsilan

(Bis-acetoxymethyl)-butyl-methylsilan

Refernces