ETHYL METHYL SULFONE

Base Information

• Chemical Name: ETHYL METHYL SULFONE
• CAS No.: 594-43-4
• Molecular Formula: C3H8O2S
• Molecular Weight: 108.161
• Hs Code.: 2930909899
• Mol file: 594-43-4.mol

Synonyms:Sulfone,ethyl methyl (6CI,7CI,8CI);Ethyl methyl sulfone;Methyl ethyl sulfone;

Chemical Property of ETHYL METHYL SULFONE

Chemical Property:

• Vapor Pressure: 0.0629mmHg at 25°C
• Melting Point: 34 °C
• Refractive Index: 1.413
• Boiling Point: 239.2 °C at 760 mmHg
• Flash Point: 120.8 °C
• PSA: 42.52000
• Density: 1.091 g/cm³
• LogP: 1.13170

Purity/Quality:

98%,99%, ^*data from raw suppliers

Ethyl methyl sulfone ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 43
• Safety Statements: 24/25-36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL METHYL SULFONE

There total 36 articles about ETHYL METHYL SULFONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-diacetylaminobenzene (10268-78-7) → 2,4-diaminonitrobenzene (5131-58-8)

Guidance literature:

With nitric acid; acetic acid; und Verseifen mit konz.Natronlauge;

Reference yield:

7-chloro-6-nitro-4(3H)-quinazolinone (53449-14-2) → 2-hydroxy-4-amino-1-nitrobenzene (16292-86-7) + 2,4-diaminonitrobenzene (5131-58-8) + 2,4-diamino-5-nitro-benzoic acid (81946-23-8)

Guidance literature:

With ammonium hydroxide; In butan-1-ol; at 175 ℃; for 24h;

Reference yield:

2,5-dinitroaniline (619-18-1) → 2,4-diaminonitrobenzene (5131-58-8)

Guidance literature:

With pyridine; hydrogen sulfide; ammonia; at 100 ℃;

upstream raw materials:

Ethyl methyl sulfide

2-(ethanesulfonyl)acetic acid

ethyl β,β-dichlorovinyl sulfone

ethylmagnesium bromide

Downstream raw materials:

2-ethanesulfonyl-1-o-tolyl-ethylideneamine

methanesulfonamide

Ethanesulfonamide

2-ethanesulfonyl-1-phenyl-ethylideneamine

Refernces

• 1、 Fawcett, Allan H.,Fee, Sean,Stuckey, Michael,Walkden, Peter. "The vibrational spectra and rotational isomerism of methyl ethyl sulphone-d0, -d3 and -d5". . p. 797 - 804. Retrieved 1987.
• 2、 Zhou, Qingqing,Ye, Man,Ma, Wenbao,Li, Difan,Ding, Bingjie,Chen, Manyu,Yao, Yefeng,Gong, Xueqing,Hou, Zhenshan. "Ionic Liquid Stabilized Niobium Oxoclusters Catalyzing Oxidation of Sulfides with Exceptional Activity". . p. 4206 - 4217. Retrieved 2019/03/26.
• 3、 Lu, Jingkun,Wang, Yaping,Ma, Xinyi,Niu, Yanjun,Singh, Vikram,Ma, Pengtao,Zhang, Chao,Niu, Jingyang,Wang, Jingping. "Synthesis and characterization of a Sb(v)-containing polyoxomolybdate serving as a catalyst for sulfoxidation". . p. 8070 - 8077. Retrieved 2018/06/29.