Technology Process of 1,1'-dibenzyl-1,1',2,2',3,3',4,4'-octahydro-6,6'-biquinoline
There total 3 articles about 1,1'-dibenzyl-1,1',2,2',3,3',4,4'-octahydro-6,6'-biquinoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert-butylammonium hexafluorophosphate(V);
In
acetonitrile;
at 20 ℃;
for 6h;
Electrochemical reaction;
DOI:10.1016/j.tetlet.2021.153021
- Guidance literature:
-
With
diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; (meta-(trifluoromethyl)phenyl)boronic acid;
In
1,2-dichloro-ethane;
at 60 ℃;
for 12h;
DOI:10.1021/acs.orglett.1c00302
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / 120 °C
2: iron(III) chloride hexahydrate / toluene / 8 h / 85 °C
With
iron(III) chloride hexahydrate; potassium carbonate;
In
toluene; acetonitrile;
DOI:10.1021/jo4002504