Technology Process of 4-benzoylbenzaldehyde dimethyl acetal
There total 3 articles about 4-benzoylbenzaldehyde dimethyl acetal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1,1-dimethoxy-1-(4-bromophenyl)methane;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 - -50 ℃;
for 0.666667h;
N,N-dimethylbenzamide;
In
tetrahydrofuran; hexane;
at -78 - 0 ℃;
DOI:10.1021/jo102309w
- Guidance literature:
-
With
potassium phosphate; PdCl(NH2C6H4C6H4)(C6H4(CH3)4O3PC6H5); water;
In
2-methyltetrahydrofuran;
at 60 ℃;
for 20h;
Inert atmosphere;
DOI:10.1021/ja2064318
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis(η3-allyl-μ-chloropalladium(II)); triethyl phosphite / 12 h / 100 °C
2: potassium phosphate; PdCl(NH2C6H4C6H4)(C6H4(CH3)4O3PC6H5); water / 2-methyltetrahydrofuran / 20 h / 60 °C / Inert atmosphere
With
potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); PdCl(NH2C6H4C6H4)(C6H4(CH3)4O3PC6H5); water; triethyl phosphite;
In
2-methyltetrahydrofuran;
DOI:10.1021/ja2064318
