2-Methylbenz[c,d]indole

Base Information

• Chemical Name: 2-Methylbenz[c,d]indole
• CAS No.: 40484-49-9
• Molecular Formula: C12H9N
• Molecular Weight: 167.21
• Hs Code.: 2933990090
• Mol file: 40484-49-9.mol

Synonyms:2-Methyl-1-azaacenaphthylene;

Chemical Property of 2-Methylbenz[c,d]indole

Chemical Property:

• Vapor Pressure: 0.00285mmHg at 25°C
• Refractive Index: 1.658
• Boiling Point: 294.446 °C at 760 mmHg
• Flash Point: 123.785 °C
• PSA: 12.36000
• Density: 1.161 g/cm³
• LogP: 2.72950
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

2-Methylbenz[cd]indole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2-Methylbenz[cd]indole is a derivative of 1-Acetamidonaphthalene (A158455) and is used in the synthesis of benzo[c,d]indole-based dimethine cyanine dyes which serve as an OFF-ON-OFF type of pH fluorescent sensor.

Technology Process of 2-Methylbenz[c,d]indole

There total 2 articles about 2-Methylbenz[c,d]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

1-nitro-8-naphthaleneethanone → 2-methyl-1-azaacenaphthylene (40484-49-9)

Guidance literature:

With ZrO₂/H₂SO₄; hydrogen; In water; N,N-dimethyl-formamide; at 25 ℃; for 6h; under 750.075 Torr; Solvent; Autoclave;

Reference yield:

→ 2-methyl-1-azaacenaphthylene (40484-49-9)

Guidance literature:

entspr. 1-Acylaminonaphthalan, POCl3;

DOI:10.1007/BF00476146

Refernces

• 1、 -. "Preparing method of 2-methyl benzo-[c,d]benzpyrole". Paragraph 0018. . Retrieved 2016/11/02.