Dicyclopropyldisulfide

Base Information

• Chemical Name: Dicyclopropyldisulfide
• CAS No.: 68846-57-1
• Molecular Formula: C6H10S2
• Molecular Weight: 146.277
• Mol file: 68846-57-1.mol

Synonyms:Dicyclopropyldisulfide;

Chemical Property of Dicyclopropyldisulfide

Chemical Property:

• Refractive Index: 1.614
• Boiling Point: 217.1 °C at 760 mmHg
• Flash Point: 132.2 °C
• PSA: 50.60000
• Density: 1.22g/cm³
• LogP: 2.69260

Purity/Quality:

98%,99%, ^*data from raw suppliers

DICYCLOPROPYLDISULFIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dicyclopropyldisulfide

There total 1 articles about Dicyclopropyldisulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopropanethiol (6863-32-7) → (cyclopropyldisulfanyl)cyclopropane (68846-57-1)

Guidance literature:

With iodine;

DOI:10.1021/ja00491a063

Reference yield: 91.0%

(cyclopropyldisulfanyl)cyclopropane (68846-57-1) + (R)-4-bromo-N-(6-(2-methylmorpholino)pyridin-2-yl)-2-(6-azaspiro[2.5]octan-6-yl)benzamide → (R)-4-(cyclopropylthio)-N-(6-(2-methylmorpholino)pyridin-2-yl)-2-(6-azaspiro[2.5]octan-6-yl)benzamide

Guidance literature:

With n-butyllithium; dibutylmagnesium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;

Reference yield: 71.0%

(cyclopropyldisulfanyl)cyclopropane (68846-57-1) → cyclopropanesulfonyl chloride (139631-62-2)

Guidance literature:

With acetic anhydride; chlorine; at 5 ℃; for 12h;

DOI:10.1021/ja00035a050

upstream raw materials:

cyclopropanethiol

Downstream raw materials:

cyclopropanesulfonyl chloride

Refernces

• 1、 Block, Eric,Schwan, Adrian,Dixon, David A.. "In Pursuit of Cyclopropanethione: Cyclopropanethione S-Oxide and S,S-Dioxide". . p. 3492 - 3499. Retrieved 2007/10/02.