N-phenyliodonio α-phenylacetamide tosylate

Base Information

• Chemical Name: N-phenyliodonio α-phenylacetamide tosylate
• CAS No.: 106266-43-7
• Molecular Formula: C₇H₇O₃S*C₁₄H₁₃INO
• Molecular Weight: 509.365
• Mol file: 106266-43-7.mol

Synonyms:N-phenyliodonio α-phenylacetamide tosylate

Chemical Property of N-phenyliodonio α-phenylacetamide tosylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-phenyliodonio α-phenylacetamide tosylate

There total 1 articles about N-phenyliodonio α-phenylacetamide tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

benzene (75067-08-2) + Benzeneacetamide (103-81-1) → N-phenyliodonio α-phenylacetamide tosylate (106266-43-7)

Guidance literature:

In acetonitrile; for 0.0166667h; Product distribution; Ambient temperature; other amides;

DOI:10.1021/jo00379a039

Reference yield: 81.0%

N-phenyliodonio α-phenylacetamide tosylate (106266-43-7) → benzylamine p-toluenesulfonic acid (14613-34-4)

Guidance literature:

With water; In acetonitrile; for 0.5h; Product distribution; Heating; other N-phenyliodonio amide tosylates; other reaction time;

DOI:10.1021/jo00379a039

Reference yield: 69.0%

dimethylsulfide (75-18-3) + N-phenyliodonio α-phenylacetamide tosylate (106266-43-7) → iodobenzene (591-50-4) + C10H14NOS(1+)*C7H7O3S(1-) (120188-88-7)

Guidance literature:

In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1016/S0040-4039(00)96746-7

upstream raw materials:

benzene

Benzeneacetamide

Downstream raw materials:

iodobenzene

C₁₀H₁₄NOS⁽¹⁺⁾*C₇H₇O₃S^(1-)

ethyl N-benzylcarbamate

benzylamine p-toluenesulfonic acid

Refernces