Piperazine ferulate

Base Information

• Chemical Name: Piperazine ferulate
• CAS No.: 171876-65-6
• Molecular Formula: C₁₈H₂₆O₄
• Molecular Weight: 306.402
• Hs Code.: 2933599090
• Mol file: 171876-65-6.mol

Synonyms:2-Ethylhexyl-3-(4-hydroxy-3-methoxyphenyl)acrylate;

Chemical Property of Piperazine ferulate

Chemical Property:

• Boiling Point: 425.791 °C at 760 mmHg
• PKA: 8?+-.0.20(Predicted)
• Flash Point: 144.915 °C
• PSA: 90.82000
• Density: 1.061 g/cm³
• LogP: 1.33540

Purity/Quality:

99% ^*data from raw suppliers

Piperazine Ferulate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Piperazine ferulate

There total 5 articles about Piperazine ferulate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-(4-hydroxy-3-methoxyphenyl)acrylic acid (1135-24-6,537-98-4) + 2-Ethylhexyl alcohol (104-76-7) → ferulic acid (2-ethylhexyl) ester (171876-65-6)

Guidance literature:

at 50 ℃; for 120h;

Reference yield: 98.0%

2-Ethylhexyl acrylate (103-11-7) + 2-methoxy-4-propenylphenol (97-54-1) → (E)-2-ethylhexyl ferulate (171876-65-6)

Guidance literature:

With Hoveyda-Grubbs catalyst first generation; In 1,2-dichloro-ethane; at 70 ℃; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1021/ja310054d

Reference yield: 72.0%

→ (E)-2-ethylhexyl ferulate (171876-65-6)

Guidance literature:

upstream raw materials:

3-(4-hydroxy-3-methoxyphenyl)acrylic acid

2-Ethylhexyl alcohol

2-Ethylhexyl acrylate

2-methoxy-4-propenylphenol

Refernces

• 1、 Higman, Carolyn S.,De Araujo,Fogg, Deryn E.. "Tandem catalysis: Versus one-pot catalysis: Ensuring process orthogonality in the transformation of essential-oil phenylpropenoids into high-value products via olefin isomerization-metathesis". . p. 2077 - 2084. Retrieved 2016.
• 2、 -. "METHOD FOR PRODUCING CINNAMIC ACID ESTER COMPOUND". Paragraph 0066-0067; 0070; 0075. . Retrieved 2020/05/06.