3,4-Diaminobenzhydrazide

Base Information

• Chemical Name: 3,4-Diaminobenzhydrazide
• CAS No.: 103956-09-8
• Molecular Formula: C7H10N4O
• Molecular Weight: 166.183
• Hs Code.: 2928000090
• European Community (EC) Number: 626-414-7
• DSSTox Substance ID: DTXSID10403987
• Wikidata: Q82207917
• Mol file: 103956-09-8.mol

Synonyms:3,4-Diaminobenzhydrazide;3,4-diaminobenzohydrazide;103956-09-8;3,4-Bis(Azanyl)benzohydrazide;SCHEMBL1252657;3,4-Diaminobenzhydrazide, 97%;DTXSID10403987;YGCXQTYRSKMILM-UHFFFAOYSA-N;Benzoic acid,3,4-diamino-,hydrazide;MFCD00017069;AKOS005171612;AS-58471;CS-0204858;D4551;FT-0614197;E83894;A896330;J-001073;L99

Chemical Property of 3,4-Diaminobenzhydrazide

Chemical Property:

• Appearance/Colour: brown solid
• Melting Point: 157-161 °C(lit.)
• Refractive Index: 1.705
• PKA: 12.88±0.10(Predicted)
• PSA: 107.16000
• Density: 1.367 g/cm³
• LogP: 1.70810
• XLogP3: -1.5
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 166.08546096
• Heavy Atom Count: 12
• Complexity: 173

Purity/Quality:

98%,99%, ^*data from raw suppliers

3,4-Diaminobenzhydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1C(=O)NN)N)N

Technology Process of 3,4-Diaminobenzhydrazide

There total 1 articles about 3,4-Diaminobenzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,4-diaminobenzohydrazide (103956-09-8)

Guidance literature:

Reference yield: 89.0%

3,4-diaminobenzohydrazide (103956-09-8) → 2-phenyl-5-(5-phenyl-1,3,4-oxadiazole-2-yl)-1H-benzo[d]imidazole (1616086-54-4)

Guidance literature:

With Al³⁺-K₁₀ montmorillonite clay; In neat (no solvent); at 55 ℃; for 0.25h; Microwave irradiation;

DOI:10.1016/j.tetlet.2014.05.004

Reference yield: 70.0%

3,4-diaminobenzohydrazide (103956-09-8) + bis-(2,4-dihydroxythiobenzoyl)sulfinyl (344567-18-6) → 4-(5-(5-(2,4-dihydroxyphenyl)-1,3,4-thiadiazol-2-yl)-1H-benzo[d]imidazol-2-yl)benzene-1,3-diol

Guidance literature:

In methanol; Reflux;

DOI:10.1007/s11164-018-3483-0

Downstream raw materials:

2-phenyl-5-(5-phenyl-1,3,4-oxadiazole-2-yl)-1H-benzo[d]imidazole

Refernces

• 1、 -. "Methods for glycosylation inhibition using amino-benzoic acids and derivatives". . . Retrieved 2008/06/13.