HEPTYL-BETA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: HEPTYL-BETA-D-GLUCOPYRANOSIDE
• CAS No.: 78617-12-6
• Molecular Formula: C13H26O6
• Molecular Weight: 278.346
• Hs Code.: 29400000
• Mol file: 78617-12-6.mol

Synonyms:1-Heptylb-D-glucoside;Heptyl glucoside;Heptyl b-D-glucopyranoside;n-Heptyl b-D-glucopyranoside;n-Heptyl b-D-glucoside;

Chemical Property of HEPTYL-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

• Vapor Pressure: 1.03E-09mmHg at 25°C
• Melting Point: 74-75℃
• Refractive Index: 1.518
• Boiling Point: 443.1 °C at 760 mmHg
• Flash Point: 221.8 °C
• PSA: 99.38000
• Density: 1.21 g/cm³
• LogP: -0.22670
• Storage Temp.: 2-8°C

Purity/Quality:

98%, ^*data from raw suppliers

Heptyl b-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: n-Heptyl-beta-D-glucopyranoside is useful for lipid vesicle preparation and solubilization of membrane-bound proteins.

Technology Process of HEPTYL-BETA-D-GLUCOPYRANOSIDE

There total 19 articles about HEPTYL-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

n-heptyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (28245-00-3) → n-heptyl beta-D-glucopyranoside (78617-12-6)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 24h;

Reference yield: 27.0%

C20H32O11 → n-heptyl beta-D-glucopyranoside (78617-12-6)

Guidance literature:

With water; triethylamine; In methanol; at 50 ℃; for 14h;

DOI:10.1134/S1070428020100231

Reference yield: 18.0%

D-Glucose (2280-44-6) + n-heptan1ol (111-70-6) → heptyl α-D-glucopyranoside, anhydrous + n-heptyl beta-D-glucopyranoside (78617-12-6)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; Yield given;

DOI:10.1016/S0008-6215(98)00302-4

upstream raw materials:

n-heptyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

D-Glucose

n-heptan1ol

4-nitrophenyl-β-D-glucoside

Downstream raw materials:

(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-nonyloxy-tetrahydro-pyran-3,4,5-triol

β-D-glucose

n-heptan1ol

O-n-pentyl β-D-glucopyranoside

Refernces

• 1、 De Winter, Karel,Van Renterghem, Lisa,Wuyts, Kathleen,Pelantová, Helena,K?en, Vladimír,Soetaert, Wim,Desmet, Tom. "Chemoenzymatic synthesis of β-D-glucosides using cellobiose phosphorylase from Clostridium thermocellum". . p. 1961 - 1969. Retrieved 2015/06/02.
• 2、 Wang, Qinqqin,Yu, Huilei,Zhao, Na,Li, Chunxiu,Shang, Yazhuo,Liu, Honglai,Xu, Jianhe. "Significantly Improved Equilibrium Yield of Long-Chain Alkyl Glucosides via Reverse Hydrolysis in a Water-Poor System Using Cross-Linked Almond Meal as a Cheap and Robust Biocatalyst". . p. 275 - 280. Retrieved 2016/04/10.