6-BN-CAMP SODIUM SALT

Base Information

• Chemical Name: 6-BN-CAMP SODIUM SALT
• CAS No.: 32115-08-5
• Molecular Formula: C₁₇H₁₈N₅O₆P
• Molecular Weight: 419.334
• Mol file: 32115-08-5.mol

Synonyms:Adenosine,N-benzyl-, cyclic 3',5'-(hydrogen phosphate) (8CI);4H-Furo[3,2-d]-1,3,2-dioxaphosphorin, adenosine deriv.; 6-(Benzylamino)purineriboside 3',5'-monophosphate; 6-Benzylamino-3',5'-purine riboside3',5'-monophosphate; Cyclic 6-benzylamino-3',5'-PuMP; N-Benzyladenosine cyclicmonophosphate; N6-Benzyl-9-b-D-ribofuranosyladenine cyclic 3',5'-monophosphate; N6-Benzyl-cAMP;N6-Benzyl-cyclic AMP; N6-Benzyladenosine 3',5'-cyclic phosphate;N6-Benzyladenosine 3',5'-monophosphate

Chemical Property of 6-BN-CAMP SODIUM SALT

Chemical Property:

• Vapor Pressure: 9.61E-22mmHg at 25°C
• Boiling Point: 719.8 °C at 760 mmHg
• Flash Point: 389.1 °C
• PSA: 153.49000
• Density: 1.86 g/cm³
• LogP: 1.72370

Purity/Quality:

99% ^*data from raw suppliers

6-BN-CAMP SODIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-BN-CAMP SODIUM SALT

There total 4 articles about 6-BN-CAMP SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4aR,6R,7R,7aS)-2-Oxo-6-(6-{[1-phenyl-meth-(Z)-ylidene]-amino}-purin-9-yl)-tetrahydro-2λ5-furo[3,2-d][1,3,2]dioxaphosphinine-2,7-diol → N6-Benzyl-cAMP (32115-08-5,65199-05-5)

Guidance literature:

With sodium cyanoborohydride; In acetic acid; at 50 ℃; for 8h; Yield given;

DOI:10.1248/cpb.36.2212

Reference yield:

benzaldehyde (100-52-7) → N6-Benzyl-cAMP (32115-08-5,65199-05-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tri-n-butylamine / acetic acid / 0.5 h / 50 °C

2: sodium cyanoborohydride / acetic acid / 8 h / 50 °C

With tributyl-amine; sodium cyanoborohydride; In acetic acid;

DOI:10.1248/cpb.36.2212

Reference yield:

cAMP (60-92-4) → N6-Benzyl-cAMP (32115-08-5,65199-05-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tri-n-butylamine / acetic acid / 0.5 h / 50 °C

2: sodium cyanoborohydride / acetic acid / 8 h / 50 °C

With tributyl-amine; sodium cyanoborohydride; In acetic acid;

DOI:10.1248/cpb.36.2212

upstream raw materials:

benzaldehyde

cAMP

Refernces