1,3-butanedioldicarbanilate

Base Information

• Chemical Name: 1,3-butanedioldicarbanilate
• CAS No.: 75052-43-6
• Molecular Formula: C₁₈H₂₀N₂O₄
• Molecular Weight: 328.368
• Mol file: 75052-43-6.mol

Synonyms:1,3-butanedioldicarbanilate

Chemical Property of 1,3-butanedioldicarbanilate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-butanedioldicarbanilate

There total 3 articles about 1,3-butanedioldicarbanilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1.3-butanediol (18826-95-4,107-88-0) + phenyl isocyanate (103-71-9) → (+/-)-1.3-bis-phenylcarbamoyloxy-butane (75052-43-6)

Guidance literature:

DOI:10.1021/ja01175a600

Reference yield:

phenyl isocyanate (103-71-9) → 1,3-butanedioldicarbanilate (75052-43-6)

Guidance literature:

Reference yield:

ethyl acetoacetate (141-97-9) + phenyl isocyanate (103-71-9) → (+/-)-1.3-bis-phenylcarbamoyloxy-butane (75052-43-6)

Guidance literature:

Multistep reaction; (i) KBH₄, EtOH, (ii) /BRN= 471391/;

DOI:10.1039/jr9630002743

upstream raw materials:

1.3-butanediol

phenyl isocyanate

ethyl acetoacetate

Downstream raw materials:

(R)-butane-1,3-diol