GLYCEROL-13C3

Base Information

• Chemical Name: GLYCEROL-13C3
• CAS No.: 63346-81-6
• Molecular Formula: C3H8O3
• Molecular Weight: 95.0617
• Mol file: 63346-81-6.mol

Synonyms:[1,2,3-13C3]Glycerol;Glycerol-13C3;Glycerol-13C3, 99 ATOM % 13C;

Chemical Property of GLYCEROL-13C3

Chemical Property:

• Melting Point: 20 °C(lit.)
• Refractive Index: n20/D 1.474(lit.)
• Boiling Point: 182 °C(lit.)
• Flash Point: 320 °F(lit.)
• PSA: 60.69000
• Density: 1.297 g/cm³
• LogP: -1.66810
• Storage Temp.: Hygroscopic, Refrigerator, under inert atmosphere
• Solubility.: DMSO (Slightly), Methanol (Sparingly)

Purity/Quality:

98% ^*data from raw suppliers

Glycerol-13C3 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Glycerol is used both in sample preparation and gel formation for polyacrylamide gel electrophoresis. Glycerol (5-10%) increases the density of a sample so that the sample will layer at the bottom of a gel’s sample well. Glycerol is also used to aid in casting gradient gels and as a protein stabilizer and storage buffer component. This is the labeled version.

Technology Process of GLYCEROL-13C3

There total 1 articles about GLYCEROL-13C3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ [1,2,3-13C3]glycerol (63346-81-6)

Guidance literature:

Galacosylglycerol, Hydrolyse;

DOI:10.1021/ja00846a001

Reference yield: 92.0%

[1,2,3-13C3]glycerol (63346-81-6) + trityl chloride (76-83-5) → 1,3-Di-O-trityl(1,2,3-(13)C3)glycerol

Guidance literature:

With pyridine; dmap; In dichloromethane; for 18h; Ambient temperature;

DOI:10.1021/ja00117a003

Reference yield: 16.0%

2-methyl-3-phenylquinoxaline (10130-23-1) + [1,2,3-13C3]glycerol (63346-81-6) → C15(13)C3H14N2 (1400975-28-1)

Guidance literature:

2-methyl-3-phenylquinoxaline; [1,2,3-¹³C₃]glycerol; at 300 ℃; for 19h; Inert atmosphere;

With hydrogenchloride; In water; at 20 ℃; for 0.166667h;

DOI:10.1021/ol302348v

Downstream raw materials:

C₁₅⁽¹³⁾C₃H₁₄N₂

carbon dioxide

C₄⁽¹³⁾CH₉NO₂