PYRROLE-2,3,4,5-D4

Base Information

• Chemical Name: PYRROLE-2,3,4,5-D4
• CAS No.: 17767-94-1
• Molecular Formula: C₄H₅N
• Molecular Weight: 71.0586
• Mol file: 17767-94-1.mol

Synonyms:Pyrrole-2,3,4,5-d₄;

Chemical Property of PYRROLE-2,3,4,5-D4

Chemical Property:

• Boiling Point: 129.76 °C at 760 mmHg
• Flash Point: 33.333 °C
• PSA: 15.79000
• Density: 1.05 g/cm³
• LogP: 1.01470

Purity/Quality:

99%, ^*data from raw suppliers

Pyrrole-2,3,4,5-d4 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Pyrrole-2,3,4,5-d4 (CAS# 17767-94-1) is a useful isotopically labeled research compound.

Technology Process of PYRROLE-2,3,4,5-D4

There total 3 articles about PYRROLE-2,3,4,5-D4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

pyrrole (109-97-7,30604-81-0) → Pyrrole-2,3,4,5-d4 (17767-94-1)

Guidance literature:

With d⁽⁴⁾-methanol; prenyl bromide; at 28 ℃; for 16h;

DOI:10.1039/d1ob01275d

Reference yield:

pentadeuterio-pyrrole (18430-85-8) → Pyrrole-2,3,4,5-d4 (17767-94-1)

Guidance literature:

With water;

DOI:10.1063/1.1742597 DOI:10.1021/ja01259a015

Reference yield:

→ Pyrrole-2,3,4,5-d4 (17767-94-1)

Guidance literature:

Pyrrol, D2O, mit D2 gesaettigte Pd/Kohle, 100grad, 18 Std.;

DOI:10.1021/ja01082a021

upstream raw materials:

pentadeuterio-pyrrole

pyrrole

Refernces

• 1、 Darshana, Dhanushka,Sureram, Sanya,Mahidol, Chulabhorn,Ruchirawat, Somsak,Kittakoop, Prasat. "Spontaneous conversion of prenyl halides to acids: application in metal-free preparation of deuterated compounds under mild conditions". supporting information. p. 7390 - 7402. Retrieved 2021/09/07.