ALLYL-D5 BROMIDE

Base Information

• Chemical Name: ALLYL-D5 BROMIDE
• CAS No.: 102910-37-2
• Molecular Formula: C3BrD5
• Molecular Weight: 126.01
• Mol file: 102910-37-2.mol

Synonyms:Propene-1,1,2,3,3-d5,bromo- (6CI);

Chemical Property of ALLYL-D5 BROMIDE

Chemical Property:

• Boiling Point: 68.107 °C at 760 mmHg
• PSA: 0.00000
• Density: 1.46 g/cm³
• LogP: 1.56730

Purity/Quality:

99% ^*data from raw suppliers

Allyl-d5 Bromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: ALLYL-D5 BROMIDE is used as a reagent in the synthesis of Resveratrol derivatives. Resveratrol (R150000) is a minor constituent of wine, correlated with serum lipid reduction and inhibition of platelet aggregation.

Technology Process of ALLYL-D5 BROMIDE

There total 3 articles about ALLYL-D5 BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

1,2,3-Tribromoperdeuteropropan (102910-32-7) → allyl bromide-d5 (102910-37-2)

Guidance literature:

With magnesium; In diethyl ether; for 0.5h; Ambient temperature;

DOI:10.1055/s-1985-31344

Reference yield:

Propiolsaeure (3634-35-3) → allyl bromide-d5 (102910-37-2)

Guidance literature:

With lithium aluminium deuteride; ethyl [2]alcohol; hydrogen bromide; Yield given. Multistep reaction; 1.) ether, 5 deg C, 12 h, 2.) reflux, 15 min;

DOI:10.1055/s-1985-31344

Reference yield:

→ allyl bromide-d5 (102910-37-2)

Guidance literature:

Hexadeuteropropen, Br2;

DOI:10.1139/v61-043

upstream raw materials:

Propiolsaeure

1,2,3-Tribromoperdeuteropropan

Downstream raw materials:

N-(5-hexynyl)-N-allyl-d5-L-alanine methyl ester

Benzyl-2,6-didesoxy-3-O-(perdeuterallyl)-α-L-ribo-hexopyranosid

Benzyl-2,6-didesoxy-4-O-(perdeuteroallyl)-α-L-ribo-hexopyranosid

Refernces