HEXANEDIOIC-3,3,4,4-D4 ACID

Base Information

• Chemical Name: HEXANEDIOIC-3,3,4,4-D4 ACID
• CAS No.: 121311-78-2
• Molecular Formula: C₆H₁₀O₄
• Molecular Weight: 150.111
• Mol file: 121311-78-2.mol

Synonyms:(3, 3, 4, 4-²H₄)Hexanedioic acid;

Chemical Property of HEXANEDIOIC-3,3,4,4-D4 ACID

Chemical Property:

• Boiling Point: 338.539 °C at 760 mmHg
• Flash Point: 172.745 °C
• PSA: 74.60000
• Density: 1.285 g/cm³
• LogP: 0.71600
• Storage Temp.: Refrigerator
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

AdipicAcid-d4(Major) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Hexanedioic-3,3,4,4-d4 Acid is the labeled version of A291590. Adipic Acid is primarily used in the synthesis of nylon. It has been used as a reagent in the solid-state polymerization of nylon analogs.

Technology Process of HEXANEDIOIC-3,3,4,4-D4 ACID

There total 2 articles about HEXANEDIOIC-3,3,4,4-D4 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H22(2)H4O8 → 2,2,3,3-d4-1,4-Butandicarbonsaeure (121311-78-2)

Guidance literature:

With oxonium;

DOI:10.1002/oms.1210240304

Reference yield:

→ 2,2,3,3-d4-1,4-Butandicarbonsaeure (121311-78-2)

Guidance literature:

entspr. Dinitril, H2SO4 (S.71);

DOI:10.1021/ja00834a013

Reference yield:

methanol (67-56-1) + 2,2,3,3-d4-1,4-Butandicarbonsaeure (121311-78-2) → 3,3,4,4-tetradeuterio-hexanedioic acid dimethyl ester (55724-08-8)

Guidance literature:

With hydrogenchloride; In water; for 16h; Reflux;

Downstream raw materials:

3,3,4,4-tetradeuterio-hexanedioic acid dimethyl ester

Refernces

• 1、 Mueller, Dieter R.,Domon, Bruno,Blum, Wolfgang,Richter, Wilhelm J.,Reiner, Hartmut,et al.. "Functional Group Interaction in the Fragmentation of Protonated 2,7-Octanedione". . p. 157 - 163. Retrieved 1989.