4-Nitro-benzenesulfonic acid; compound with phenylamine

Base Information

• Chemical Name: 4-Nitro-benzenesulfonic acid; compound with phenylamine
• CAS No.: 13798-51-1
• Molecular Formula: C₆H₅NO₅S*C₆H₇N
• Molecular Weight: 296.304
• Mol file: 13798-51-1.mol

Synonyms:4-Nitro-benzenesulfonic acid; compound with phenylamine

Chemical Property of 4-Nitro-benzenesulfonic acid; compound with phenylamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-Nitro-benzenesulfonic acid; compound with phenylamine

There total 10 articles about 4-Nitro-benzenesulfonic acid; compound with phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) + (indan-2-yl) 4-nitrobenzenesulfonate → indan-2-yl anilide (33237-72-8) + 4-Nitro-benzenesulfonic acid; compound with phenylamine (13798-51-1)

Guidance literature:

In methanol; at 55 ℃; Rate constant;

DOI:10.1039/P29930002415

Reference yield:

methyl 4-nitrobenzenesulfonate (6214-20-6) + aniline (62-53-3) → 4-Nitro-benzenesulfonic acid; compound with phenylamine (13798-51-1) + N-methylaniline (100-61-8)

Guidance literature:

In methanol; at 65 ℃;

Reference yield:

4-Nitrobenzenesulfonic acid ethyl ester (15481-55-7) + aniline (62-53-3) → N-ethyl-N-phenylamine (103-69-5) + 4-Nitro-benzenesulfonic acid; compound with phenylamine (13798-51-1)

Guidance literature:

In methanol; at 65 ℃;

upstream raw materials:

methyl 4-nitrobenzenesulfonate

aniline

neopentyl 4-nitrobenzenesulfonate

4-Nitrobenzenesulfonic acid ethyl ester

Refernces

• 1、 Koh, Han Joong,Lee, Hai Whang,Lee, Ikchoon. "Bimolecular Nucleophilic Substitution (SN2) Reactions of Neopentyl Arenesulfonates with Anilines and Benzylamines in Methanol". . p. 253 - 258. Retrieved 2007/10/02.
• 2、 Lee, Ikchoon,Lee, Young Sook,Huh, Chul,Lee, Hai Whang,Lee, Byung Choon. "Nucleophilic Substitution Reactions of Indan-2-yl Arenesulfonates with Anilines in Methanol". . p. 2415 - 2418. Retrieved 2007/10/02.