N-hydroxyheptanimidamide

Base Information

• Chemical Name: N-hydroxyheptanimidamide
• CAS No.: 99623-07-1
• Molecular Formula: C₇H₁₆N₂O
• Molecular Weight: 144.217
• Hs Code.: 2925290090
• Mol file: 99623-07-1.mol

Synonyms:N'-hydroxyheptanimidamide;

Chemical Property of N-hydroxyheptanimidamide

Chemical Property:

• Boiling Point: 264.3 °C at 760 mmHg
• Flash Point: 113.6 °C
• PSA: 56.11000
• Density: 1 g/cm³
• LogP: 2.40350

Purity/Quality:

99%, ^*data from raw suppliers

N-HYDROXYHEPTANIMIDAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-hydroxyheptanimidamide

There total 2 articles about N-hydroxyheptanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

heptanenitrile (629-08-3) → 1-Imino-hydroxyamino-heptan (99623-07-1)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In ethanol;

DOI:10.1021/jm00314a017

Reference yield:

heptanenitrile (629-08-3) → heptanamide oxime (99623-07-1)

Guidance literature:

With hydroxylamine;

Reference yield:

heptanamide oxime (99623-07-1) + 1-(triphenylmethyl)-5-(methyloxycarbonyl)-1,4,5,6-tetrahydropyrimidine (146422-24-4) → 5-(3-Hexyl-[1,2,4]oxadiazol-5-yl)-1-trityl-1,4,5,6-tetrahydro-pyrimidine (1026226-77-6)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, a) 0 deg C, 15 min, b) reflux, 45 min, 2.) THF, reflux, 18 h;

DOI:10.1021/jm00059a008

upstream raw materials:

heptanenitrile

Downstream raw materials:

5-(3-Hexyl-[1,2,4]oxadiazol-5-yl)-1-trityl-1,4,5,6-tetrahydro-pyrimidine