2-NITRO-1-NAPHTHYLAMINE

Base Information

• Chemical Name: 2-NITRO-1-NAPHTHYLAMINE
• CAS No.: 607-23-8
• Molecular Formula: C10H8N2O2
• Molecular Weight: 188.186
• Hs Code.: 2921450090
• Mol file: 607-23-8.mol

Synonyms:1-Naphthylamine,2-nitro- (7CI,8CI);1-Amino-2-nitronaphthalene;2-Nitro-1-naphthylamine;NSC167919;

Chemical Property of 2-NITRO-1-NAPHTHYLAMINE

Chemical Property:

• Vapor Pressure: 2.57E-06mmHg at 25°C
• Melting Point: 143 °C(Solv: ethanol (64-17-5))
• Refractive Index: 1.728
• Boiling Point: 390.8 °C at 760 mmHg
• PKA: -1.53±0.10(Predicted)
• Flash Point: 190.2 °C
• PSA: 71.84000
• Density: 1.366 g/cm³
• LogP: 3.43460

Purity/Quality:

99% ^*data from raw suppliers

2-Nitro-1-naphthalenamine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-NITRO-1-NAPHTHYLAMINE

There total 3 articles about 2-NITRO-1-NAPHTHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

1-amino-naphthalene (134-32-7) → 2-nitro-1-naphthylamine (607-23-8) + 1-amino-4-nitronaphthalene (776-34-1)

Guidance literature:

With bromine; silver nitrate; triphenylphosphine; In acetonitrile; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tetlet.2006.07.054

Reference yield:

N-(2-nitronaphthalen-1-yl)acetamide (2437-30-1) → 2-nitro-1-naphthol (607-24-9) + 2-nitro-1-naphthylamine (607-23-8)

Guidance literature:

With potassium hydroxide; at 110 ℃;

Reference yield:

1-acetamidonaphthalene (575-36-0) → 2-nitro-1-naphthylamine (607-23-8) + 1-amino-4-nitronaphthalene (776-34-1)

Guidance literature:

With water; nitric acid; acetic acid; Behandeln des Reaktionsprodukts mit Chlorwasserstoff in Methanol;

DOI:10.1021/ja01341a029

upstream raw materials:

N-(2-nitronaphthalen-1-yl)acetamide

1-acetamidonaphthalene

1-amino-naphthalene

Downstream raw materials:

(2-nitro-[1]naphthyl)-bis-(toluene-4-sulfonyl)-amine

nitrobenzene

1-phenyl-2-aminonaphthalene

2-nitro-1-phenylnaphthalene

Refernces

• 1、 Bagal,Luchkevich,El'tsov. "Transformations of Diazonium Salts. III. Transformations, Acid-Base Properties, and Reactivity of Nitronaphthyldiazonium Salts". . p. 119 - 132. Retrieved 2007/10/03.