1-isocyanato-6-methoxycarbonylaminohexane

Base Information

• Chemical Name: 1-isocyanato-6-methoxycarbonylaminohexane
• CAS No.: 13590-53-9
• Molecular Formula: C₉H₁₆N₂O₃
• Molecular Weight: 200.238
• Mol file: 13590-53-9.mol

Synonyms:1-isocyanato-6-methoxycarbonylaminohexane

Chemical Property of 1-isocyanato-6-methoxycarbonylaminohexane

Chemical Property:

Purity/Quality:

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Technology Process of 1-isocyanato-6-methoxycarbonylaminohexane

There total 1 articles about 1-isocyanato-6-methoxycarbonylaminohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.1%

1,6-bis(methoxycarbonylamino)hexane (6030-54-2) → 1-isocyanato-6-methoxycarbonylaminohexane (13590-53-9) + Hexamethylene diisocyanate (822-06-0,28182-81-2,28574-90-5,88357-62-4)

Guidance literature:

With dibutyltin dilaurate; 3-(3-methyl-1H-imidazol-3-ium-1-yl)propane-1-sulfonate; at 240 ℃; for 2h; under 20 Torr; Temperature; Reagent/catalyst; Pressure;

upstream raw materials:

1,6-bis(methoxycarbonylamino)hexane

Refernces

• 1、 Ammar, Muhammad,Cao, Yan,He, Peng,Wang, Li-Guo,Chen, Jia-Qiang,Li, Hui-Quan. "Zn-Co bimetallic supported ZSM-5 catalyst for phosgene-free synthesis of hexamethylene–1,6–diisocyanate by thermal decomposition of hexamethylene–1,6–dicarbamate". . p. 1583 - 1589. Retrieved 2017.