N-Methyldipropylamine

Base Information

• Chemical Name: N-Methyldipropylamine
• CAS No.: 3405-42-3
• Molecular Formula: C7H17 N
• Molecular Weight: 115.219
• Hs Code.: 2921199090
• Mol file: 3405-42-3.mol

Synonyms:Dipropylamine,N-methyl- (6CI,7CI,8CI); Dipropylmethylamine; Methyldipropylamine;N,N-Dipropylmethylamine; N-Methyldipropylamine

Chemical Property of N-Methyldipropylamine

Chemical Property:

• Vapor Pressure: 18mmHg at 25°C
• Melting Point: -91.17°C (estimate)
• Refractive Index: n20/D 1.406(lit.)
• Boiling Point: 117 °C(lit.)
• Flash Point: 3 ºC
• PSA: 3.24000
• Density: 0.734
• LogP: 1.73820
• Water Solubility.: Soluble in hot water.

Purity/Quality:

99%, ^*data from raw suppliers

N-Methyldipropylamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,C
• Statements: 11-34
• Safety Statements: 16-26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Methyldipropylamine

There total 30 articles about N-Methyldipropylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.5%

(5-fluoroindol-3-yl)dimethylsulfonium perchlorate (1440957-24-3) + di-n-propylamine (142-84-7) → N-methyldipropylamine (3405-42-3) + 5-fluoro-(3-thiomethyl)-indole

Guidance literature:

for 1h; Inert atmosphere; Reflux;

DOI:10.1248/cpb.c12-00882

Reference yield: 98.1%

di-n-propylamine (142-84-7) + (1H-indol-3-yl)dimethylsulfonium perchlorate → 3-methylthioindole (40015-10-9) + N-methyldipropylamine (3405-42-3)

Guidance literature:

at 107 ℃; for 1h; Inert atmosphere;

DOI:10.1248/cpb.c12-00882

Reference yield: 96.6%

(5-methylindol-3-yl)dimethylsulfonium perchlorate (1440957-18-5) + di-n-propylamine (142-84-7) → 5-methyl-3-(methylthio)-1H-indole (40015-14-3) + N-methyldipropylamine (3405-42-3)

Guidance literature:

for 1h; Inert atmosphere; Reflux;

DOI:10.1248/cpb.c12-00882

upstream raw materials:

potassium methyl sulfate

di-n-propylamine

methyl iodide

nitromethane

Refernces

• 1、 Yu, Xiaoxiao,Yang, Zhenzhen,Zhang, Hongye,Yu, Bo,Zhao, Yanfei,Liiu, Zhenghui,Ji, Guipeng,Liu, Zhimin. "Ionic liquid/H2O-mediated synthesis of mesoporous organic polymers and their application in methylation of amines". supporting information. p. 5962 - 5965. Retrieved 2017/07/10.
• 2、 -. "SULFIDE SCAVENGERS, METHODS FOR MAKING AND METHODS FOR USING THEM". Paragraph 0069. . Retrieved 2013/07/19.