(+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane

Base Information

• Chemical Name: (+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane
• CAS No.: 775352-38-0
• Molecular Formula: C₁₇H₂₈O₃
• Molecular Weight: 280.408
• Mol file: 775352-38-0.mol

Synonyms:(+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane

Chemical Property of (+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane

There total 1 articles about (+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane (775352-38-0)

Guidance literature:

With copper oxide-chromium oxide; at 150 - 170 ℃; under 147102 Torr; Hydrogenation;

DOI:10.1021/ja01182a067

Reference yield:

(+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane (775352-38-0) → 5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene (56469-10-4)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether; potassium; carbon disulfide / Erhitzen des Reaktionsprodukts unter vermindertem Druck

2: Raney nickel / Hydrogenation

3: aqueous HBr; acetic acid

With carbon disulfide; diethyl ether; hydrogen bromide; potassium; nickel; acetic acid;

DOI:10.1021/ja01182a067

Reference yield:

(+/-)-3-hydroxy-2-methyl-2-(3.5-dimethoxy-phenyl)-octane (775352-38-0) → 1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene (60526-81-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; potassium; carbon disulfide / Erhitzen des Reaktionsprodukts unter vermindertem Druck

2: Raney nickel / Hydrogenation

With carbon disulfide; diethyl ether; potassium; nickel;

DOI:10.1021/ja01182a067

Downstream raw materials:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene