4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester

Base Information

• Chemical Name: 4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester
• CAS No.: 848599-31-5
• Molecular Formula: C₂₀H₂₃BrO₄
• Molecular Weight: 407.304
• Mol file: 848599-31-5.mol

Synonyms:4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester

Chemical Property of 4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester

There total 1 articles about 4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4,4-bis(4-hydroxyphenyl)valeric acid (126-00-1) + 1,3-dibromo-propane (109-64-8) → 4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester (848599-31-5)

Guidance literature:

4,4-bis(4-hydroxyphenyl)valeric acid; With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 80 ℃; for 0.5h;

1,3-dibromo-propane; In N,N-dimethyl-formamide; at 80 ℃; for 5h;

DOI:10.1021/ja042854f

Reference yield:

4,4-bis-(4-hydroxy-phenyl)-pentanoic acid 3-bromo-propyl ester (848599-31-5) → C37H32N4O4

Guidance literature:

Multi-step reaction with 2 steps

1.1: 40 percent / acetonitrile / 5 h / Heating

2.1: acetonitrile / 0.5 h / 75 °C

2.2: 42 percent / DBU / acetonitrile; methanol / 20 h / 75 °C

In acetonitrile;

DOI:10.1021/ja042854f

upstream raw materials:

4,4-bis(4-hydroxyphenyl)valeric acid

1,3-dibromo-propane

Refernces