C₃₉H₆₁BrO₆Si₂

Base Information

• Chemical Name: C₃₉H₆₁BrO₆Si₂
• CAS No.: 1315567-73-7
• Molecular Formula: C₃₉H₆₁BrO₆Si₂
• Molecular Weight: 761.985
• Mol file: 1315567-73-7.mol

Synonyms:C₃₉H₆₁BrO₆Si₂

Chemical Property of C₃₉H₆₁BrO₆Si₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₃₉H₆₁BrO₆Si₂

There total 8 articles about C₃₉H₆₁BrO₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C39H62O7Si2 (1315567-82-8) → C39H61BrO6Si2 (1315567-73-7)

Guidance literature:

With pyridine; dibromo sulfoxide; In diethyl ether; at -40 ℃;

DOI:10.1038/nchem.1074

Reference yield:

C18H23BrO3 → C39H61BrO6Si2 (1315567-73-7)

Guidance literature:

Multi-step reaction with 5 steps

1.1: isopropyl alcohol / 80 °C

2.1: 122 °C / neat (no solvent)

2.2: 20 °C

3.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation

4.1: iodine; magnesium / diethyl ether / 0 °C

5.1: pyridine; dibromo sulfoxide / diethyl ether / -40 °C

With pyridine; dibromo sulfoxide; iodine; magnesium; In diethyl ether; 1,2-dichloro-benzene; isopropyl alcohol; 2.1: Claisen rearrangement;

DOI:10.1038/nchem.1074

Reference yield:

C36H56O7Si2 (1315567-67-9) → C39H61BrO6Si2 (1315567-73-7)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine; magnesium / diethyl ether / 0 °C

2: pyridine; dibromo sulfoxide / diethyl ether / -40 °C

With pyridine; dibromo sulfoxide; iodine; magnesium; In diethyl ether;

DOI:10.1038/nchem.1074

upstream raw materials:

C₃₉H₆₂O₇Si₂

C₃₆H₅₆O₇Si₂

(+)-dimethyl-2,3-O-isopropylidene-D-tartrate

benzyl bromide

Downstream raw materials:

C₃₃H₅₂O₉Si

C₄₁H₄₄O₁₂

C₄₄H₄₈O₁₂

C₃₃H₄₇BrO₆Si

Refernces