2-ethyl-2-methyl-3-phenylthiohexanal

Base Information

• Chemical Name: 2-ethyl-2-methyl-3-phenylthiohexanal
• CAS No.: 344443-03-4
• Molecular Formula: C₁₅H₂₂OS
• Molecular Weight: 250.405
• Mol file: 344443-03-4.mol

Synonyms:2-ethyl-2-methyl-3-phenylthiohexanal

Chemical Property of 2-ethyl-2-methyl-3-phenylthiohexanal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-ethyl-2-methyl-3-phenylthiohexanal

There total 7 articles about 2-ethyl-2-methyl-3-phenylthiohexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

α-chlorobutyl phenyl sulfide (72653-47-5) + (Z)-dimethyl((2-methylbut-1-en-1-yl)oxy)(phenyl)silane (90121-89-4) → 2-ethyl-2-methyl-3-phenylthiohexanal (344443-03-4)

Guidance literature:

With titanium(IV) isopropylate; titanium tetrachloride; In dichloromethane; at -78 ℃; for 0.666667h;

Reference yield:

α-chlorobutyl phenyl sulfide (72653-47-5) + (E)-dimethyl((2-methylbut-1-en-1-yl)oxy)(phenyl)silane (90121-90-7) → 2-ethyl-2-methyl-3-phenylthiohexanal (344443-03-4)

Guidance literature:

With titanium(IV) isopropylate; titanium tetrachloride; In dichloromethane; at -78 ℃; for 0.666667h;

Reference yield:

(n-butylthio)benzene (1126-80-3) → 2-ethyl-2-methyl-3-phenylthiohexanal (344443-03-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / N-chlorosuccinimide / CCl₄ / 12 h / Ambient temperature

2: 84 percent / TiCl₄, Ti(OPrⁱ)4 / CH₂Cl₂ / 0.67 h / -78 °C

With titanium(IV) isopropylate; N-chloro-succinimide; titanium tetrachloride; In tetrachloromethane; dichloromethane;

upstream raw materials:

α-chlorobutyl phenyl sulfide

(Z)-dimethyl((2-methylbut-1-en-1-yl)oxy)(phenyl)silane

(E)-dimethyl((2-methylbut-1-en-1-yl)oxy)(phenyl)silane

(n-butylthio)benzene

Refernces