2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

Base Information

• Chemical Name: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE
• CAS No.: 400-67-9
• Molecular Formula: C7H4ClF3N2O2
• Molecular Weight: 240.569
• Hs Code.: 2921420090
• Mol file: 400-67-9.mol

Synonyms:o-Toluidine,6-chloro-a,a,a-trifluoro-4-nitro- (6CI,8CI);2-Chloro-4-nitro-6-trifluoromethylaniline;2-Chloro-4-nitro-6-trifluoromethylphenylamine;

Chemical Property of 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

Chemical Property:

• Vapor Pressure: 0.00272mmHg at 25°C
• Refractive Index: 1.542
• Boiling Point: 286 °C at 760 mmHg
• Flash Point: 126.7 °C
• PSA: 71.84000
• Density: 1.614 g/cm³
• LogP: 3.95360
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

98%min ^*data from raw suppliers

2-Amino-3-chloro-5-nitrobenzotrifluoride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 20/21/22-36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Amino-3-chloro-5-nitrobenzotrifluoride is a useful intermediate for the preparation of monoazo dyes.

Technology Process of 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

There total 2 articles about 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-nitro-2-trifluoromethyl-aniline (121-01-7) → 2-chloro-4-nitro-6-trifluoromethyl-aniline (400-67-9)

Guidance literature:

With N-chloro-succinimide; In acetonitrile; at 150 ℃; for 0.25h; Microwave irradiation;

Reference yield:

→ 2-chloro-4-nitro-6-trifluoromethyl-aniline (400-67-9)

Guidance literature:

2.3-Dichlor-5-nitro-benzotrifluorid, NH3 (fl.)/H2O/Et3NCl <Δ>;

upstream raw materials:

4-nitro-2-trifluoromethyl-aniline

Refernces

• 1、 -. "SUBSTITUTED MORPHOLINE AND THIOMORPHOLINE DERIVATIVES". Page/Page column 46. . Retrieved 2008/06/13.