CYANIMIDODITHIOCARBONIC ACID S-BENZYL ESTER S-POTASSIUM SALT

Base Information

• Chemical Name: CYANIMIDODITHIOCARBONIC ACID S-BENZYL ESTER S-POTASSIUM SALT
• CAS No.: 36598-30-8
• Molecular Formula: C9H8 N2 S2 . K
• Molecular Weight: 246.39
• Mol file: 36598-30-8.mol

Synonyms:Benzylpotassium cyanimidodithiocarbonate; Benzyl potassium cyanoimidodithiocarbonate;Potassium benzyl cyanodithioimidocarbonate; Potassium benzylcyanoimidodithiocarbonate

Chemical Property of CYANIMIDODITHIOCARBONIC ACID S-BENZYL ESTER S-POTASSIUM SALT

Chemical Property:

• Vapor Pressure: 0.000206mmHg at 25°C
• Melting Point: 215 °C
• Boiling Point: 327.2°C at 760 mmHg
• Flash Point: 151.7°C
• PSA: 86.75000
• LogP: 2.95438

Purity/Quality:

98%Min ^*data from raw suppliers

CYANIMIDODITHIOCARBONIC ACID S-BENZYL ESTERS-POTASSIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYANIMIDODITHIOCARBONIC ACID S-BENZYL ESTER S-POTASSIUM SALT

There total 2 articles about CYANIMIDODITHIOCARBONIC ACID S-BENZYL ESTER S-POTASSIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

benzyl bromide (100-39-0) + potassium cyanocarbonimidodithioate (13145-41-0) → cyano-dithiocarbamic acid benzyl ester; potassium salt (36598-30-8)

Guidance literature:

In acetone; at 0 - 20 ℃; for 6h;

DOI:10.1021/acs.jmedchem.7b01492

Reference yield:

→ cyano-dithiocarbamic acid benzyl ester; potassium salt (36598-30-8)

Guidance literature:

K-Salz 2, CH3Br;

DOI:10.1021/jo00943a011

Reference yield: 80.0%

2,3-bis(bromomethyl)quinoxaline (3138-86-1) + cyano-dithiocarbamic acid benzyl ester; potassium salt (36598-30-8) → 2,3-Bis<<(benzylthio)(cyanimino)methyl>thiomethyl>chinoxalin (85219-60-9)

Guidance literature:

In chloroform; acetone; for 24h; Ambient temperature;

upstream raw materials:

benzyl bromide

potassium cyanocarbonimidodithioate

Downstream raw materials:

[3-(2-nitro-phenyl)-4-oxo-thiazolidin-2-ylidene]-cyanamide

4-Amino-2-benzylthio-5-thiazol-(N,N-pentamethylencarboxamid)

3t-(4-amino-2-benzylsulfanyl-thiazol-5-yl)-acrylonitrile

3t-(4-amino-2-benzylsulfanyl-thiazol-5-yl)-acrylic acid methyl ester

Refernces