2,3,4,5,6-PENTACHLORO(TRIFLUOROMETHYL) BENZENE

Base Information

• Chemical Name: 2,3,4,5,6-PENTACHLORO(TRIFLUOROMETHYL) BENZENE
• CAS No.: 384-83-8
• Molecular Formula: C7Cl5 F3
• Molecular Weight: 318.337
• Hs Code.: 2903999090
• Mol file: 384-83-8.mol

Synonyms:Benzene,pentachloro(trifluoromethyl)- (9CI); Toluene, 2,3,4,5,6-pentachloro-a,a,a-trifluoro- (6CI,7CI,8CI); 2,3,4,5,6-Pentachloro-1-(trifluoromethyl)benzene;Pentachlorobenzotrifluoride

Chemical Property of 2,3,4,5,6-PENTACHLORO(TRIFLUOROMETHYL) BENZENE

Chemical Property:

• Melting Point: 78-82 °C
• Boiling Point: 279.0±35.0 °C(Predicted)
• Flash Point: 140oC
• PSA: 0.00000
• Density: 1.742±0.06 g/cm3(Predicted)
• LogP: 5.97240

Purity/Quality:

99% ^*data from raw suppliers

1,2,3,4,5-Pentachloro-6-trifluoromethyl-benzene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3,4,5,6-PENTACHLORO(TRIFLUOROMETHYL) BENZENE

There total 4 articles about 2,3,4,5,6-PENTACHLORO(TRIFLUOROMETHYL) BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

trichlorofluoromethane (75-69-4) + octachlorotoluene (2605-69-8) → 2,3,4,5,6-pentachloro-1-(trifluoromethyl)benzene (384-83-8)

Guidance literature:

With aluminium trichloride; for 7h; ice bath;

DOI:10.1021/jo00001a022

Reference yield: 77.0%

trichlorofluoromethane (75-69-4) + pentachlorobenzene (608-93-5) → 2,3,4,5,6-pentachloro-1-(trifluoromethyl)benzene (384-83-8)

Guidance literature:

With aluminium trichloride; Ambient temperature;

DOI:10.1016/S0040-4039(01)80668-7

Reference yield:

4-chlorobenzotrifluoride (98-56-6) → 2,3,4,5,6-pentachloro-1-(trifluoromethyl)benzene (384-83-8)

Guidance literature:

With chlorosulfonic acid;

upstream raw materials:

α,α,α-trifluorotoluene

trichlorofluoromethane

pentachlorobenzene

octachlorotoluene

Downstream raw materials:

octachlorotoluene

pentachlorobenzoyl chloride

pentachlorobenzoyl fluoride

perchlorobenzoic acid

Refernces

• 1、 Castaner, J.,Riera, J.,Carilla, J.,Robert, A.,Molins, E.,Miravitlles, C.. "A New Trifluoromethylating Agent: Synthesis of Polychlorinated (Trifluoromethyl)benzenes and 1,3-Bis(trifluoromethyl)benzenes and Conversion into Their Trichloromethyl Counterparts and Molecular Structure of Highly Strained Polychloro-m-xylenes". . p. 103 - 110. Retrieved 2007/10/02.